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GCMS analysis results for sample AD31641, February 2002

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GCMS analysis report for sample AD31641 conducted on February 11, 2002.

NYC-WTC_000049745–000049761

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02

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NYC 9/11 Public Portal Document

A LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\JAN0302\31641.D Vial: 39 Acq On : 4 Jan 2002 11:32 pm Operator: 209 GALOS Sample : gems scan l/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.465 260 264 275 rBV 312513 821157 14.89% 2.904% 2 7.603 275 279 298 rVB2 68128 279477 5.07% 0.988% 3 11.523 701 706 727 rBV 1651325 4241541 76.90% 15.002% 4 14.167 987 994 999 rBV 37352 74573 1.35% 0.264% 5 15.122 1092 1098 1117 rBV 2597779 5389018 97.70% 19.061%

6 20.391 1666 1672 1687 rBV 2617770 5515998 100.00% 19.510% 7 24.807 2147 2153 2166 rBV2 2421781 5216100 94.56% 18.449% 8 24.954 2166 2169 2188 rVB 18568 61496 1.11% 0.218% 9 29.884 2701 2706 2711 rBV 321382 609483 11.05% 2.156% 10 32.831 3021 3027 3046 rBV2 1436620 3317558 60.14% 11.734%

11 34.364 3189 3194 3203 rBV2 24163 73093 1.33% 0.259% 12 35.245 3283 3290 3300 rBV 38263 129087 2.34% 0.457% 13 36.108 3379 3384 3397 rBV 49772 174859 3.17% 0.618% 14 36.898 3463 3470 3478 rBV 810376 2127733 38.57% 7.526% 15 36.999 3478 3481 3499 rVB4 41808 180052 3.26% 0.637%

16 38.027 3585 3593 3598 rBV5 15724 61794 1.12% 0.219%

Sum of corrected areas: 28273019

31641.D GCMS1126.M Fri Feb 01 11:16:22 2002

NYC-WTC_000049750

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NYC-WTC_000049750Source: NYC Law Department, mirrored locally

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