GCMS reference analysis results for sample AE08684, April 22, 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR2202\REF1.D Vial: 4 Acq On : 22 Apr 2002 12:05 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 22 14:51 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.21 152 477535 20.00 ug/1 -0.03 10) Naphthalene-d8 15.85 136 1740332 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 985176 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.59 188 1477129 20.00 ug/1 -0.03 39) Chrysene-dl2 33.65 240 998502 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 610986 20.00 ug/1 -0.05

System Monitoring Compounds 28) TCMX 23.29 209 44920 9.10 ug/L -0.04 Spiked Amount 10.000 Recovery = 91.00% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.87 74 98035 9.43 ug/1 99 3) bis(2-Chloroethyl)ether 11.60 93 243461 15.05 ug/1 99 4) 1,3-Dichlorobenzene 12.11 146 209823 12.58 ug/1 99 5) 1,4-Dichlorobenzene 12.26 146 217427 12.95 ug/1 99 6) 1,2-Dichlorobenzene 12.77 146 216959 13.92 ug/1 99 7) 2,2’-oxybi s(1-Chioropropan 13.09 45 338915 15.16 ug/1 99 8) N-Nitroso-di-n-propylamine 13.48 70 157069 14.81 ug/1 99 9) Hexachloroethane 13.62 117 64692 10.52 ug/1 98 11) Nitrobenzene 13.89 77 220530 14.45 ug/1 99 12) Isophorone 14.54 82 365322 12.65 ug/1 98 13) bis(2-Chloroethoxy)methane 15.22 93 291985 15.53 ug/1 99 14) 1,2,4-Trichlorobenzene 15.73 180 186971 14.13 ug/1 98 15) Naphthalene 15.90 128 652096 15.58 ug/1 99 16) Hexachlorobutadiene 16.45 225 69257 10.47 ug/1 99 18) Hexachlorocyclopentadiene 18.65 237 8567 1.97 ug/1 # 90 19) 2-Chloronaphthalene 19.41 162 396061 15.24 ug/1 97 20) Dimethylphthalate 20.49 163 519320 17.34 ug/1 99 21) 2,6-Dinitrotoluene 20.71 165 107350 14.99 ug/1 93 2 2) Acenaphthylene 20.67 152 586688 16.14 ug/1 99 23) Acenaphthene 21.24 153 420286 16.26 ug/1 100 24) 2,4-Dinitrotoluene 21.88 165 140134 14.86 ug/1 99 25) Diethylphthalate 22.63 149 493225 17.17 ug/1 100 26) 4-Chlorophenyl-phenylether 22.79 204 225113 17.66 ug/1 97 27) Fluorene 22.76 166 470369 17.19 ug/1 98 29) Azobenzen/ 1,2-Diphenylhyd 23.24 77 431155 14.18 ug/L 97 31) N-Nitrosodiphenylamine 23.17 168 150075 12.21 ug/1 98 32) 4-Bromophenyl-phenylether 24.25 248 126491 17.64 ug/1 95 (#) = qualifier out of range (m) = manual integration REF1.D GCMS0412.M Mon Anr 22 14:53:08 2002 PAGA 1

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