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GCMS calibration results for DFTPP, April 15, 2002

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Calibration report for DFTPP standard used in GCMS analysis, generated on April 15, 2002, by operator.

NYC-WTC_000048705–000048708

Folder label: “GCMS X 4/11/02 A 4/15/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\l\DATA\APR1202\CAL10.D Vial: 2 Acq On 15 Apr 2002 9:04 am Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 16 14:44 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Apr 16 11:47:07 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 3 3) Hexachiorobenzene 24.71 284 223234 21.28 ug/1 97 3 4) Phenanthrene 25.68 178 975573 20.68 ug/1 100 35) Anthracene 25.81 178 957243 20.63 ug/1 99 36) Di-n-butylphthalate 27.58 149 1204802 20.42 ug/1 100 37) Fluoranthene 29.30 202 975069 20.55 ug/1 99 4 0) Pyrene 29.98 202 1000682 20.44 ug/1 99 41) Butylbenzylphthalate 32.11 149 463049 19.34 ug/1 98 42) Benzo(a)anthracene 33.61 228 677607 19.95 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.88 149 595544 19.44 ug/1 99 44) Chrysene 33.74 228 686393 20.38 ug/1 98 46) Di-n-Octylphthalate 35.62 149 . 847278 18.38 ug/1 99 47) Benzo(b)fluoranthene 36.72 252 600263 20.15 ug/1 98 48) Benzo(k)fluoranthene 36.79 252 571463 19.70 ug/1 98 4 9) Benzo(a)pyrene 37.71 252 476562 19.41 ug/1 99 50) Indeno(1,2,3-cd)pyrene 42.00 276 479012 19.37 ug/1 98 51) Dibenz(a,h)anthracene 42.08 278 368915 19.57 ug/1 98 52) Benzo(g,h,i)perylene 43.23 276 410954 19.91 ug/1 99

(#) = qualifier out of range (m) = manual integration CAL10.D GCMS0412.M Tue Apr 16 14:46:20 2002 Page 2

NYC-WTC_000048707

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NYC-WTC_000048707Source: NYC Law Department, mirrored locally

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