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GCMS blank results for volatile organics, April 2002

Machine-extracted title · confidence 100%

Laboratory report showing blank analysis results for volatile organic compounds in sample AE08260 from April 2002.

NYC-WTC_000048225–000048255

Folder label: “GCMS X 4/9/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020417\0409LB.D Vial: 4 Acq On 17 Apr 2002 11:51 am Operator: Nefliu Sample 04/09 1b Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 Benzoic acid, 2-(1-oxopropyl)- Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

30.58 0.72 ug/L 734903 Chrysene-dl2 30.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzoic acid, 2-(1-oxopropyl)- 178 C10H10O3 002360-45-4 38 2 Benzoic acid, 2-(1-oxopropyl)- 178 C10H10O3 002360-45-4 38 3 1,2-Benzenedicarboxylic acid, bu... 304 C18H24O4 000084-64-0 38 4 1,2-Benzenedicarboxylic acid, di... 362 C22H3404 003648-21-3 33 Abundance Scan 4680 (30.577 min): 0409LB.D (-4675) (-) m/z 149.00 100.00% 149

5000- 57 99 167 265 AM 30.20 30.40 30 60 30 80 31.00

n/z—> 0 I1 111 I'1 0 20 40 36,70183 1111 129......... . 60 I 80 100 120 140 160 180 200 I 220 240 260 m/z 57.10 29.86% Abundance #66791 Benzoic acid. 2-(1 -oxopropyl) 149

U 5000 30 20 30.40 30.60 30.80 31.00 85 m/z 99.10 22.99% 27 50 . 77 93 105 121 1‘IT it T 1T‘ TTI । r11 0—1 । ।15> • । । T । ..95133 । r । । ■« T । । t । । i 161 178 n/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #123454: Benzoic acid, 2-(1-oxopropyl)- 149

30 20 30.40 30.60 30.80 31 00 5000- m/z 54.10 11.76% 65 51 77 93 105 121133 n/z-> 4 0- T' • । • । ■ ■ ■ ■ । । • rt | r» 0 20 40 60 < f I t 11 । । । 1‘ । r । । । 161 178 80 100 120 140 160 180 200 220 240 260 Abundance #66736' 1,2-Benzenedicarboxylic acid, butyl cyclohexyl ester 149 Bpoomotrur 111/4.91 30 20 30.40 30.60 30 80 31 00 m/z 96.10 11.23% 5000

29 41 55 67 ,83 0 -----TT—TITTITTPTT 104 121 135 167 205 223 *1.11)11., III. |(l. n/z- > 0 20 40 60 80 100 120 140 160 180 200 220 240 260 30.20 30.40 30 60 30.80 31 00

0409LB.D 041702SCAN.M Thu Apr 18 09:42:00 2002 Page 15

NYC-WTC_000048242

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NYC-WTC_000048242Source: NYC Law Department, mirrored locally

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