GCMS results sample AE08212, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1702\8212.D Vial: 23 Acq On : 18 Apr 2002 5:42 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Benzoic acid, phenyl ester Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

33.35 1.26 ug/1 144350 Chrysene-dl2 33.64

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Benzoic acid, phenyl ester 198 C13H10O2 000093-99-2 35 2 .beta.-D-Ribofuranose, 1-acetate 2, 504 C28H2409 006974-32-9 35 3 1,2-Bis(benzoyloxy)benzene 318 C20H14O4 000643-94-7 35 4 2 - Bromo isobjutyrophenone 226 ClOHllBrO 010409-54-8 35 Abundance Scan 3083 (33.345 min): 8212.D (-) m/z 104.90 100.00% 105 149

5000 77 । -1 | । i r ’l | P I I | ITT I 1 1 "n I | i

51 163 33.00 33.20 33.40 33.60 ......... J....... , 122 I 207 83.34% III I I I I I I I I 1 I r i ■1111 ■ ■ ‘' i11' ■ i ■ ■ ■11'1 r 11' ■1 r i ■''11' ‘ ■ ■ i ■111111111111111111111 m/ Z 149.00 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #22451: Benzoic acid, phenyl ester 105

T I | I I I I | I — I | I T“I I | I I—I i- i 5000 77 33.00 33.20 33.40 33.60 m/z 77.05 39.56% 51 198 . I . 122 141 i i I’t" < I . II111 I TH p-1 r. | . I 1 | > . i | i i i |”I I < I |“f i I i | I I I I | | i r r | r r

m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #59067: .beta.-D-Ribofuranose, 1 -acetate 2,3,5-tribenzoate 105 • 1 i ’ ’ T 33.00 33.20 33.40 33.60 5000 m/ z 51.00 9.22% 77

51 122 .i 201 322 i ' ' ■ ' i ' ' i 1 i1 r ■ ■ i1 '1' i 1 ■ ■ ■ i 1 '1 ' i'1 '11''1 ■ i' 1 '' i' 11 11'''' i1 ' ’' 111111 1ITTI" 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #45379:1,2-Bis(benzoyloxy)benzene ..... .................. ■ 1 । ''', । 1 1 ' 1 । 1 1 1 1 r1 1 1 1 i 1 105 33.00 33.20 33.40 33.60 m/z 150.00 8.13%

5000 77

27 51 1 121 137 197 213 318 \...... A....... | ' '' ' 1 | 1 | । |I 1■ ‘‘111|1 ‘‘ ' 1 | ‘ | 1 । 1 । | ' ' ' ' | 1 1 ' 1 | ‘ 111111111 | 11..... 1'1111111111111111*1′111 ■ ■ i ■ ■ ■ ■ । ■ ' । ■ ■ ■ ■ । 1 1 1 1 i ' /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 33.00 33.20 33.40 33.60

8212.D GCMS0412.M Thu Apr 18 14:12:09 2002 Page 1

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