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GCMS blank analysis AE08209, April 2002

Machine-extracted title · confidence 100%

GCMS blank analysis report for sample AE08209 listing volatile organic compounds from April 2002.

NYC-WTC_000047955–000047966

Folder label: “GCMS X 4/8/02 A 4/18/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\APR17 02\LBA.D Vial: 16 Acq On 17 Apr 2002 10:52 pm Operator: Sample gc/ms scan 4/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 2-Nitro-4-(trifluoromethyl)phe Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

45.40 0.57 ug/1 42677 Perylene-dl2 37.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Nitro-4-(trifluoromethyl) phenol 207 C7H4F3NO3 000400-99-7 9 2 trans-3-Ethoxy/.beta.-methyl-.beta. 207 C11H13NO3 000000-00-0 9 3 Silane, trimethyl [5-methyl-2-(1-met 222 C13H22OSi 055012-80-1 9 4 Benzenamine, 4-bromo-2-chloro- 205 C6H5BrClN 038762-41-3 9 Abundance ( Scan 4395 (45.397 min): LBA.D (-) m/z 73.00 100.00%

_A__ 73 207 147

5000 281 355

327 429 45.00 45.20 45.40 45.60 45.80

m/z—> 44 l ............. I .............. !.......... I ur m/z 207.00 H | i i ■ I | I I I I | | i I | | | | | i | i । | । । 1 । । | | f I I I | I I | । | | | | i

20 40 60 80 100120140160180200220240260280300320340360380400420 TTTTp-rrrpm-q- 83.59% Abundance #24493: 2-Nitro-4-(trifluoromethyl)phenol wwMwWWWwopyhp 207

A 63 T-j-r-r-r-T-j-r-T 5000 113 45.00 45.20 45.40 45.60 45.80 30 132 161 m/z 147.00 77.84% 83 188 I I TTTTTTTTTTT i" " i" " i 'lH"l TT m/z—> 20 40 60 80 100120140160180200220240260280300320340 360 380 400420 Abundance #24563: trans-3-Ethoxy-.beta.-methyl-.beta.-nitrostyrene 207 I ‘ 11 ‘I 'I I I I I I I I I 11111/1/1 45.00 45.20 45.40 45.60 45.80 5000 77 103 131 m/z 221.05 71.86% 162

I I | r " 111 H ■ i TT ‘ ‘8 ‘ ‘11 i "I m/z-> 20 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #70609: Silane, trimethyl[5-methyl-2-(1-methylethyl)phenoxy T‘1 1 ■1 r1 11 1 i 73 207 45.00 45.20 45.40 45.60 45.80 m/z 281.00 44.90% 5000 WMWAuy 45 .. 165 1 r"'r'" i TTTTTTTTTTTTTTTTTTT I""i m/z—> 20 40 60 80 100120140160180200220240260 280 300 320340 360 380 400420 45.00 45.20 45.40 45.60 45.80

LBA.D GCMS0412.M Thu Apr 18 14:13:51 2002 Page 5

NYC-WTC_000047965

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NYC-WTC_000047965Source: NYC Law Department, mirrored locally

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