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GCMS analysis results for sample AE07978, Apr 2002

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Laboratory report documenting the GCMS analysis of sample AE07978 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046707–000046721

Folder label: “GCMS X 4/5/02 A 4/16/02

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Scanned page image, NYC-WTC_000046718
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020415\07978 .D Vial: 18 Acq On : 16 Apr 2002 12:44 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 2-Propanone, 1,1,1-trichloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.04 0.68 ug/L 591182 1,4-Dichlorobenzene-d4 9.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 42 2 2-Pentanone, 5-(1,2-propadienylo... 140 C8H12O2 055702-69-7 9 3 5-Iodopentan-2-one 212 C5H9IO 003695-29-2 9 4 3,6-Octadecadiynoic acid, methyl... 290 C19H30O2 056554-43-9 9 Abundance Scan 503 (6 035 min) 07978.D (-499) (-) m/ z 43.30 100.00% 45

5000

N.., ......... 59 83 97 125 5.60 5.80 6 00 6 20 6 40 O1 .............. 1 14 , , , "* , ,n. , , , " II. ....... ......... ...... m/z 125.10 7.69% n/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #3877 2-Propanone. 1,1,1-trichloro- 43

5000 5.60 5.80 6 00 6.20 6.40 m/z 127.20 7.12%

n/z-> 0- 5 27 +53.63. -- 20 40 60 73 ITT 83

80 97,110 125 ........... 100 120 140 160 180 200 Abundance #7039: 2-Pentanone, 5-(1,2-propadienyloxy) 43 ________ 5.60 5.80 6.00 6 20 6.40 5000 m/z 59.30 6.37% 85 15 27 .

n/z—> 0- 4I--- 20 40 55 60 69 80 97 । 100 112 125 120 140 140 160 180 200 - Abundance #7057 5-lodopentan-2-one i ■ 1 1 ■ i ' 43 5.60 5.80 6.00 6 20 640 m/z 83.20 5.81% 5000 85

n/z-> 0 —| 20 40 58 69 60 80 | 99 ... 127 141 155 169 100 120 140 160 180 197 213 200 5.60 M 5 80 6 00 6.20 6.40

07978.D 041202SCAN.M Tue Apr 16 13:47:47 2002 Page 8

NYC-WTC_000046718

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NYC-WTC_000046718Source: NYC Law Department, mirrored locally

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