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GCMS analysis results for sample AE09585, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09585 conducted on May 17, 2002.

NYC-WTC_000046284–000046293

Folder label: “GCMS X 5/7/02 A 5/9/02

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Scanned page image, NYC-WTC_000046292
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0802\9585.D Vial: 18 Acq On 9 May 2002 3:12 am Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.80 2.54 ug/1 211737 Naphthalene-d8 15.82

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 Noradrenaline , tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 3 Benzoic/acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 4 Phenet lamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 37 Abundance Scan 1065 (14.796 min): 9585.D (-) m/z 73.10 100.00% 73

5000- 267 355 JI ' ’ 45 14.40 14.60 14.80 15.00 15.20 i । 108 133154 193 223 323 — 1 “ r" ■■ ■ i- । । ‘ 11* । TlT ——--h TI TTT m/z 355.10 35.89% m/z—> 50 100 150 200 250 300 350 400 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 T | | | | I | I I I 4 | + 5000 14.40 14.60 14.80 15.00 15.20 m/z 267.05 35.51% 207 - । 323 I m/z-> 50 100 150 200 250 300 350 400 Abundance #57357: Noradrenaline, tetra-TMS 73 .................. ............. .............. I | I I I I | I I I I | I ! I I | I 1 I 1 | I ’

14.40 14.60 14.80 15.00 15.20 5000 102 355 m/z 356.10 11.76

45 147 442 1 ri l r m/z—> 50 100 150 200 250 300 350 400 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet ................... < । । । i i [ i i i i । । । । । । n ir । i r \.......... ........... 73 14.40 14.60 14.80 15.00 15.20 m/z 268.05 9.36%

5000 355 45 133 193 223 281 I Tl 1 1 1 i ■ 1—1 r i ' 1 ■ ■ i ' '' ' 1 i 1 rI 1 i *' 1 1 1 i ' . .............. ...................... ................ m/z-> 50 100 150 200 250 300 350 400 14.40 14.60 14.80 15.00 15.20

9585.D GCMS0507.M Fri May 10 08:22:27 2002 Page 2

NYC-WTC_000046292

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NYC-WTC_000046292Source: NYC Law Department, mirrored locally

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