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GCMS analysis results for sample AE10811, May 2002

Machine-extracted title · confidence 50%

Gas chromatography-mass spectrometry report for sample AE10811 showing detection of unknown compounds and surrogate recovery.

NYC-WTC_000046036–000046063

Folder label: “GCMS X 5/7/02 A 5/15/02

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NYC 9/11 Public Portal Document

. Data File C:\MSDCHEM\1\DATA\051402\10811.D Vial : 21 Acq On 15 May 2002 6:39 am Operator: Mclean Sample 5/7 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L ********************************************************************* Peak Number 13 Phenethylamine, N-methyl-.b... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

20.68 0.77 ug/L 1056450 Acenapthalene-dlO 18.57

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 35 2 Benzeneethanamine, N-[(pentafluo... 563 C24H34F5NO3Si3 055429-13-5 35 3 Noradrenaline tetraTMS 457 C20H43NO3S14 068595-65-3 32 4 Benzoic acid, 2,4-bis[(trimethyl... 370 C16H30O4Si3 010586-16-0 32 Abundance Scan 2996 (20.682 min): 10811 D (-2984) (-) m/z 73.10 100.00% 73

5000 147 355 221 281 ..... A... 401 20.40 20.60 20.80 21.00 45 01 P H7 191 । 249, , 1 1 1327 14 1 i" ' m/z 355.10 34.48% Td‘‘‘1I*+/1111‘II4 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #115313: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethy... 73

................. / \...................... 5000 355 20.40 20.60 20.80 21.00 44 m/Z 147.10 32.40% 116 147 193220 267294 384 01 —+4 ‘I Hh ir T— , i । r > i ' 1 i ' ■ ' ' i ' ■ 1 ' i 1 1 1 ' i 1 ■ ' 1 i 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #115316: Benzeneethanamine, N-[(pentafluorophenyl)methylen... 73 355 ..... A) ' 1 । 1 1 ' ■ । 1 ' ' 20.40 20.60 20.80 21.00 5000 m/z 221.10 27.34%

45 — 117 147 179207 251,281 386 429 458 548 0- r n1dr —hepa +* | i-1- fhfi i 1 1 1 1 i ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #27959: Noradrenaline tetraTMS , .......... ... 73 20.40 20.60 20.80 21.00 m/z 281.10 20.16%

5000 102 355

45 147 0-PPm— ' ' I_| _____________________________________ 1 1 1 1 U ' 1 1 I ' 1 1 1 1 1 1 1 ’ 1 1 442 ...........H............ | > | । । i r | i i i । | i 'I i ■ | । i

m/z-> 50 100 150 200 250 300 350 400 450 500 550 20.40 20.60 20.80 21.00

10811.D 050102.M Thu May 16 14:13:26 2002 Page 17

NYC-WTC_000046057

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NYC-WTC_000046057Source: NYC Law Department, mirrored locally

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