GCMS analysis results for sample AE10810, May 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\051402\10810.D Vial: 20 Acq On : 15 May 2002 5:50 am Operator: Mclean Sample : 5/7 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 18 Dodecane, 2-cyclohexyl- Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

36.62 0.42 ug/L 370827 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dodecane, 252 2-cyclohexyl- C18H36 013151-82-1 9 2 2-(1-Piperidino)-5-nitropyridine 207 C10H13N3O2 026820-61-1 5 3 1H-Pyrrole, 2,3-dihydro-1-methyl- 83 C5H9N 033838-11-8 5 4 2-Ethoxy-1-methyl-6-oxo-1,2-azap. . . 191 C7H14NO3P 093989-00-5 5 Abundance Scan 5709 (36.623 min): 10810.D (-5706) (-) m/z 207.10 100.00% 44 82 191 207 vwuMwy“Nnyw/WMethph 147 5000 70

I I I I I I I I t l I-1 y ! I I I I I I 97 36.20 36.40 36.60 36.80 37.00 0'........... I ‘I 11 1 11 ' U ,I.............. ■ i ■ ■ ■ ■ । - ■ ■ ■ । _ ■ i ■ ■ ■ ■ i ■ ■ • ■ i > । ■ ' i ■ ■ ■ ■ i ■ ■ ■ ■ i m/ z 82.05 83.91% m/z->_____ 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #32558: Dodecane, 2-cyclohexyl- 82 55

5000 41 69 111 L 36.20 36.40 36.60 36.80 37.00 m/z 190.90 75.34% 29

m/z-> 0- — 20 40 1—r 'I i pl, — 60 80I L 97 i, 125 140 153 168 252 1——— 1 i 1 ■ ' 1 i 1 ' 1 ■ i ' ■ ' 1 i 1 ' ' 1 i 100 120 140 160 180 200 220 240 y Abundance #84816: 2-(1 -Piperidino)-5-nitropyridine 207 178 36.20 36.40 36.60 36.80 37.00 124 5000 84 m/z 44.10 71.31% 164 42 56 I 69 139 152 192 MushyvMbypwyhsM 0- TII , , pl ,141/8,-4— | Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #32306: 1H-Pyrrole, 2,3-dihydro-1-methyl- 42 82 36.20 36.40 36.60 36.80 37.00 m/z 147.00 58.45%

5000 67

55

0..2— — +-------- AA .Of Uh, A MAA Aj | । ' i I ] I I i i [ । i । 1 । 1 1 i 1 [ T I I

m/z-> 20 401 60 80I 100 120 140 160 180 200 220 240 36.20 36.40 36.60 36.80 37.00

10810.D 050102.M Thu May 16 12:40:03 2002 Page 22

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