GCMS analysis results for sample AE10702, May 20 2002

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Data File : C:\MSDCHEM\l\DATA\020513\10702.D Vial: 13 Acq On : 14 May 2002 12:24 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 10 2-Pentenoic acid, 2-[(tert-... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

40.07 0.34 ug/1 36522 Chrysene-dl2 39.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentenoic acid, 2-[/tert-butyl... 344 C17H3603Si2 1000221-74-3 10 2 Furo[2,3-c]pyridine, 2,7-dimethyl- 147 C9H9NO 069022-77-1 10 3 (3-Methoxyphenyl)acetonitrile 147 C9H9NO 019924-43-7 10 4 (2-Methoxyphenyl)acetonitrile 147 C9H9NO 007035-03-2 9 Abundance Scan 6295 (40.066 min): 10702.D (-6290) (-) m/ z 73.10 100.00% 73

147 221 5000 287 M , phn,Ahaal, । Maw, Muahpap 239 355 39 57 111 39.80 40.00 40.20 40.40 ... LLH m/z 147.00 59.71% /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #26963:2-Pentenoic acid, 2-[(tert-butyldimethylsilyl)oxy]... 73 147

5000 44 1. 1A I ’ ' 'I 39.80 40.00 40.20 40.40 41 57 189 287 m/ Z 221.00 55.01% .... 11,1.199 117 L I 173 231 257 i fI I > r i p n i p . . . 1*1 i I | > ■ ■ ■ | r t 329 —mumupuunn m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #65810: Furo[2,3-c]pyridine, 2,7-dimethyl- 147 ' 1 1 1 1 f । ■ 1 । ‘‘ 39.80 40.00 40.20 40.40 m/z 287.10 34.13% 5000

, 51 78 118 ...........111i ..... I .......... I........i '111'' " i' " ' i " 1111 " ' i' 1" i ‘" i1' " i " ‘11 " '' r " ' i' ' i1 ■ " i' " ' i " " r 1" r ' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #123310: (3-Methoxyphenyl)acetonitrile 147 39.80 40.00 40.20 40.40 m/z 74.00 29.97%

5000 77

116 51 15,314444 ‘W——*B—*2B*‘*/*A‘‘A‘‘AA‘‘I}‘‘‘‘AA‘1IA‘‘UIA** m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 39.80 40.00 40.20 40.40

10702.D SCAN020507 .M Wed May 15 08:44:14 2002 Page 12

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