GCMS analysis results for sample AE10520, May 2002

NYC 9/11 Public Portal Document Library searen compound Report

Data File : C:\HPCHEM\1\DATA\MAY1002\10520.D Vial: 43 Acq On : 12 May 2002 7:02 am Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 38.72 1.65 ug/1 80743 Perylene-dl2 37.84 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane, 1,1, 1,5,5,5-hexamethyl 3 84 C12H3 604Si5 003555-47-3 35 2 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 28 3 3-1 sopropoxy—1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17 4 3-(3-Hydroxyp henyl)-3-hydroxypropio 398 C18H3404Si3 000000-00-0 12 Abundance Scan 3676 (38.724 min): 10520.D (-) m/z 73.10 100.00% 73

147 5000 221 281 355 11 429 38.40 38.60 38.80 39.00 t 45 ! 1 i ri r—| i i j 1 1 p 1 r i j- 193 253 1 3271, 1 i 1 1 ' 1 i ' 1 1 1 i 1 1 1 ' i ' 1 m/z 147.05 52.77% m/z-> 50 100 150 200 250 300 350 400 450 500 550 __ Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147

i i । i i i r | i I I | | J-! ! I ।1 r i L 5000 281 38.40 38.60 38.80 39.00 m/z 221.10 39.05% 45 369 117 249.T - 207I I I — ' 1 i 1 1 TCT ‘ 15 I I I I I I I m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73 I I | I i ‘ I | I I I I । 1 I r ■ 1 i • 1 1 1 i 38.40 38.60 38.80 39.00 207 5000 147 m/z 281.00 22.35%

m/z-> Abundance 34

50

73 103

100 150 200 250 281 . I I 300 #60503:3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 350 395

400 482 ‘ 1111’41’ 450 500 550 _A_ 1 1 i 1 ‘ 1 1 i ' 1 ' 1 i 1 1 1 ' i 1 1 1 ' I 38.40 38.60 38.80 39.00 m/ z 355.10 21.77%

5000 147

m/z—> 1 1 | k' ' 50 T 100 kl । 1. 20027121 150 । ' > I 327 415 d r—I I | 519 561 I I | 250 300 350 400 450 500 550 I । | I1 r 1—|—I—I—।—I—| "I ।—।—[—I—।—r—1—I—P—I—[—I—r TTI ‘ ‘‘I 38.40 38.60 38.80 39.00

10520.D GCMS0510.M Thu May 16 15:45:05 2002 Page 3

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