GCMS analysis results for unknown compounds, sample AE10200, May 2002

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Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10200 on May 10, 2002.

NYC-WTC_000044942–000044958

Folder label: “GCMS X 4/30/02 A 5/8/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\10200.D Vial: 18 Acq On 9 May 2002 5:16 am Operator: Mclean Sample 4/30 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 8 Histamine, N-boc-4-chloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 34.99 0.31 ug/L 220205 Perylene-dl2 34.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Histamine, N-boc-4-chloro- 245 C10H16C1N3O2 1000128-82-9 9. 2 Oxazolidine, 2-ethyl-2-methyl- 115 C6H13NO 017026-89-0 9 3 2-Naphthalenemethanol, 1-(dimeth... 265 C17H31NO 056701-22-53 4 Bendazol 208 C14H12N2 000621-72-7 7 Abundance Scan 5431 (34.990 min): 10200.D (-5429) (-) m/z 207.00 100.00% 116 207

5000 44 84 128 259 281 Ws/WuqvaM 34.60 34.80 35.00 35.20 35.40 01 I ' ' 1 1 i ■ ■ 1 1 i ■ 1 1 ■ i 1 1 1 ' i 1 m/z 116.00 88.08% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #52005: Histamine, N-boc-4-chloro- 57 16

5000 189 । [ । i" । I । iT t| । ' > ' T i—।—i'" । ।

41 1 30 34.60 34.80 35.00 35.20 35.40 172 245 m/z 84.10 73.46% i 81 102 , 146 | 211 01 ------- TT I I I I ’ I I I I I I ।1 I 1 ' " t 1 i ■ ■ 1 ■ i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #33827: Oxazolidine, 2-ethyl-2-methyl- 84 44 34.60 34.80 35.00 35.20 35.40 5000 m/Z 86.00 68.08% 29 t 15 0- 1 | 1 I 1 —4—44 7hith./ 70 100 . 1151 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #33735: 2-Naphthalenemethanol, 1-(dimethylamino)-1,2,3,4,4... TI" 4AAAA4A,AP 411 4* M / 43 58 71 84 34.60 34.80 35.00 35.20 35.40 164 98 265 m/z 28 0.90 64.62% 114 5000

0 4 -। OU 142 | 178 I 0, , I'1! , UI1 r/A , — 192 206

, | 232 250 Aph 1 1 i 1 ' ‘ I* /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 | 34.60 34.80 35.00 35.20 35.40

10200 .D 050102.M Thu May 09 13:36:35 2002 Page 11

NYC-WTC_000044957

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GCMS analysis results for unknown compounds, sample AE10198, May 2002 · Box DEP Box 25

NYC-WTC_000044885

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10198 on May 10, 2002.

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