GCMS analysis results for unknown compounds, sample AE10204, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050802\10204.D Vial: 22 Acq On 9 May 2002 8:31 am Operator: Mclean Sample 4/30 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 Acetamide, 2-chloro-N,N-di-... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 34.99 0.25 ug/L 158794 Perylene-dl2 34.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetamide, 2-chloro-N,N-di-2-pro... 173 C8H12C1NO 000093-71-0 9 2 5,6-Dimethyl-1,3-oxathiane 132 C6H120S 114288-74-3/5 3 2-Pentanone, 4-mercapto-4-methyl- 132 C6H120S 019872-52-7 3 4 Delachlor 283 C15H22C1NO2 024353-58-0 3 Abundance Scan 5432 (34.995 min): 10204.D (-5430) (-) m/z 131.80 100.00% 49 132 96 207 5000

263 । l i i । Fl । । ] । i i i । 1 । । i—l r

281 34.60 34.80 35.00 35.20 35.40 01 1 ' I 1 1 1 1 I T”! [ l I I I | I I I | ! I I I [ I f “I I Illi ] I t I I I I I I I I III I I I I I-1 I I’l“l I [ I I I I I I m/ z 49.10 98.77% m/z-> Abundance 20

28 40

41 56 60 80 100 120 140 160 180 200 220 240 #108461: Acetamide, 2-chloro-N,N-di-2-propenyl- 260 280

IyrMsMMMs 70 5000 15 .IT ' 1 i 11 i ■ ■ ■ ■ । । ■

132 34 60 34.80 35.00 35.20 35.40 96 m/z 96.00 67.90%

o1 T7 +H■I M-r1 । T 4l——Lu 03 110 1145158 173 I II | III i | I I CT | I T ■ ■ । i i i ■ II ■ । i 11 i r। J i r

Tl/Z-> 20 40) 60 80 100 120 140 160 180 200 220 240 260 280 I Abundance #59544: 5,6-Dimethyl-1,3-oxathiane 132

34.60 34.80 35.00 35.20 35.40 60 88 5000 m/z 207.00 61.11%

0- 73

ull— 102 1 ■ i 1 1 ■ ' i 1 1 li> । । । । । | ............................................................................ iiii B i i " i i i C । ! । i । । i-1 k i i-1 i । i r AlynlMAAsh m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #4054: 2-Pentanone, 4-mercapto-4-methyl- | I I F I TI I i | | I I I | | I i i [ | | 43 34.60 34.80 35.00 35.20 35.40 m/z 209.00 58.64%

5000

29 ii 59 75 89 132 0 1 ' i r r1' ■ ... . , l ................................... ........................ 1 । i | i i i * j i i i f i I i i । । । n । । । । i p r r ■ 1 ' I1 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20 35.40

10204.D 050102.M Thu May 09 13:38:29 2002 Page 10

NYC-WTC_000045008