GCMS analysis results for unknown compounds, sample AE10200, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\10200.D Vial: 18 Acq On 9 May 2002 5:16 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Allyl O-nitrophenyl sulphide Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

34.93 0.28 ug/L 198225 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Allyl O-nitrophenyl sulphide 195 C9H9NO2S 1000146-07-6 9 2 1H-Indene, 3-methyl- 130 C10H10 000767-60-2 5/ 3 4-Phosphorinanone, 1-methyl- 130 C6H11OP 016327-48-3/5 4 1H-Indene, 1-methyl- 130 C10H10 000767-59-8 5 Abundance Scan 5421 (34.931 min): 10200.D (-5420) (-) m/z 130.20 100.00% 130

5000 264 118 43 1 ’ I fl I I I I 11 I I I I I I I I 1—I—I—P

34.60 34.80 35.00 35.20 73 191 I, 0— i ।' । r i ~ i ' । ■ |'■ । i i । । i r TH ■ । । i । i । | i l । ] । । 'i । । । i । I | । ! i i i “ rm- m/z 264.20 47.39% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #58909: Allyl O-nitrophenyl sulphide 130

106 5000 1 I | Ti l | i i I i | ) i i । । । i 41 34.60 34.80 35.00 35.20 !47 195 m/ z 12 9.40 46.13% i 01 1+11**’11111 111 1 ‘ 1 1‘ ‘I‘ TIT ■ । 1 1 । 1 । 1 1 ' । । 1 < । 1 । 1 । । । । । । ' । । । m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #121916:1H-lndene, 3-methyl- 130 115 34.60 34.80 35.00 35.20 5000 m/z 118.00 40.13%

77 91 102 O'............... I‘ ' 41 hp 1, all 146....................................... I | । Il । [ I i r । l i । । ] । । ii । । rm i l । । । । iiir "I 151

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #121925: 4-Phosphorinanone, 1 -methyl- I ' I )I 11 .......................... I I I I I ■ I" I I I I I ErI I I [ 130 34.60 34.80 35.00 35.20 m/ z 131.20 39.65%

5000 74

45 57 102 115 ,, if Tiii i , , AA AAA, n-> 0 ‘ 1411 ' ।1'1 40 60 80 100 i i

120 । । > । i

140 | 1l । ।

160 । n । ■

180 । i i i ।

200 । i 1 i

220 ] riiiTI i

240 i i r i' i—r

260 ' i 1 1 ' 1 i 1 34.60 34.80 35.00 35.20 1 ' I ' 1 ’ 1 1

10200.D 050102.M Thu May 09 13:36:35 2002 Page 10

NYC-WTC_000044956