Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.
NYC-WTC_000044650–000044656Folder label: “GCMS X 4/29/02 A 5/3/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
‘ Data File : C:\HPCHEM\1\DATA\APR2502\9333.D Vial: 10 Acq On : 25 Apr 2002 9:28 pm Operator: Sample : gc/ms scan 4/18 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 26 7:462002 1Quant Results File: GCMS0412.RES
Quant Method C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) P Title 209 625/TCLP calibration table DV ARP Last Update Thu Apr 25 15:21:43 2002 -( 0 A Response via Initial Calibration DS • A • DataAcq Meth GCMS0412 ogrP
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.21 152 673507 20.00 ug/1 -0.03 10) Naphthalene-d8 15.85 136 2467783 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 1394416 20.00 ug/1 -0.03 30) Phenanthrene-diO 25.59 188 2060394 20.00 ug/1 -0.03 39) Chrysene-dl2 33.65 240 1300663 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 801905 20.00 ug/1 -0.05
System Monitoring Compounds 8.5 7 2 8) TCMX 23.28 209 47930 6- 80- ug/L -0.05 Spiked Amount 10.000 Recovery = 68.00% SS7 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.44 74 107 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.89 128 284 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.44 165 604 N.D. 25) Diethylphthalate 22.62 149 1393 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D.
(#) = qualifier out of range (m) = manual integration 9333.D GCMS0412.M Fri Apr 26 07:46:51 2002 Page 1
NYC-WTC_000044650
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NYC-WTC_000044621
Calibration scan report for EPA Method 625 showing retention times and deviations for deuterated standards on April 25 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044700
Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.
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Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043678
Calibration table for GC/MS analysis listing deuterated standards and their response values from April 24, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044748
Calibration data file listing standard compounds and response factors for TCLP testing from late April 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043726
Calibration data for GC/MS analysis of surrogate compounds including dichlorobenzenes and naphthalene from April 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023076
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023171
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023327
Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09578 analyzed in May 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023122
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023148
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023345
Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09518 analyzed in May 2002.
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