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← Document results/DEP Box 25/GCMS X 4/25/02 A 5/7/02
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GCMS analysis results, sample AE09971, May 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE09971 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000044071–000044093

Folder label: “GCMS X 4/25/02 A 5/7/02”

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NYC 9/11 Public Portal Document

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Data File C:\MSDCHEM\1\DATA\050602\9977.D Vial: 19 Acq On 7 May 2002 2:22 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 13 2-Chloroaniline-5-sulfonic .. Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T. 36.49 0.23 ug/L 131067 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Chloroaniline-5-sulfonic acid 207 C6H6C1NO3S 000098-36-2 9 2 Quinoline, 8-bromo- 207 C9H6BrN 016567-18-3/5 3 4-Bromo-2,6-difluoroaniline 207 C6H4BrF2N 067567-26-4 5 4 trans-2,3-Methylenedioxy-b-methy ... 207 C10H9NO4 086029-47-2 5 Abundance Scan 5686 (36.488 min): 9977. D (-5684) (-) m/z 207.00 /L00.00%

8000 40 73 133 147 191 207 221 uMMb/MWMMMMMWe 6000

4000 1 ' i 1 1 1 1 i 1 1 1 1 i 1 ■ ■ 1 i 1 1 36.20 36.40 36.60 36.80 m/ Z 73.05

rra । 1 * 1 1 i 1 1 ■ ■ i ' 1 1 1 i ' ■ 1 1 i 1 1 1 1 i 1 1 ■ ■ i 1 1 1 ■ i 1 ' ' ■ i 1 1 1 ■ i 1 1 83.10% m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #84878: 2-Chloroaniline-5-sulfonic acid 207

5000 - > II I I I I I I I v I < I I I ( 111 Ttr 36.20 36.40 36.60 36.80 43 m/z 40.10 78.87% 55 90 ...........| i ' 1 1 ' i 1 L60—E 80 69 80 1100 114 126 ■i■■‘'i''■ 1।■'1 I-1 , 145................ .I,...... | I ( I I | I i I > | । I r i ] ill grd

m/z-> 20 40 100 140 120160 180 200 220 Abundance #84881: Quinoline, 8-bromo- 207 128 36.20 36.40 36.60 36.80 5000 m/z 221.00 77.46% 101 50 64 75

m/z-> TTT 20 40 27 39 _l I-'-"1' ' lll. ' ' 80 91 100 117 | 142 154 171 184 1 ‘ IU TIT > ■ । 1 l ■ 1 ' T ।11 । । । । ■ ■ I 1 ' 120 140 160 180 200 220 I Abundance #85328: 4-Bromo-2,6-difluoroaniline .......Il 11 1 1 1 1 1 1 ' 209 36.20 36.40 36.60 36.80 m/ Z 190.90 76.76% 5000

31 44 57,68 81

+93.., . । , 108 128

160 179189 — —————————— a I 1 * । 1 1 "tf m/z-> 20 40 60 80 100 120 140 160 180 200 220 36.20 36.40 36.60 36.80

9977.D 050102.M Tue May 07 15:54:25 2002 Page 17

NYC-WTC_000044092

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GCMS analysis results, sample AE09968, May 2002 · Box DEP Box 25

NYC-WTC_000043938

Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997

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