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GCMS analysis results, sample AE09771, May 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE09771 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000043893–000043918

Folder label: “GCMS X 4/25/02 A 5/7/02

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Scanned page image, NYC-WTC_000043916
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9771.D Vial: 24 Acq On 7 May 2002 6:25 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 16 2-Oxo-l-methyl-4,6-diphenyl... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

34.87 0.70 ug/L 368659 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Oxo-l-methyl-4,6-diphenyl-1,2-... 262 C17H14N20 021418-80-4 4 2 .alpha.-Methylstyrene 118 C9H10 000098-83-9 4 3 Bicyclo[4.2.0]octa-1,3,5-triene,.. 118 C9H10 022250-74-4 4 4 .alpha.-Methylstyrene 118 C9H10 000098-83-9 4 Abundance Scan 5411 (34.872 min): 9771 .D (-5410) (-) m/z 131.50 100.00% 111 118

5000 258 49 86 232 207 1 1 i ■' । । । [ । । i । | i । । i । । । । r 34.60 34.80 35.00 35.20 ill m/ Z 118.00 78.05% n1 ■ ।''' ■ ।1''11'''' ।1''' ।' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #53054: 2-Oxo-1-methyl-4,6-diphenyl-1,2-dihydropyrimidine T8

5000 ) 34.60 34.80 35.00 35.20 261 44 69 m/z 258.10 44.36%|

' i 1 1 ' 1 1 83103 1 1 1 1 ' 1 1 1 1 1* ‘ 1 1 1 131 185 234 | i 1 1 1 1 i 1 1 1 1 i 1 ' 1 1 I 1 1 1 1 I ' 1 1 1 I 1 1 1 1 I 1 1 1 1 11 1 mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #120635: .alpha.-Methylstyrene 118 ... 1 ... 34.60 34.80 35.00 35.20 5000 103 m/z 49.00 32.92% 78 20 51 91

m/z-> 27 39 1 i63 - . , ill ...1 , 111111 1 T 1 11 1 1 11 TTT 20 40 60 80 M 100 120 140 160 180 200 220 240 260 Abundance #52902: Bicyclo[4.2.0]octa-1,3,5-triene, 3-methyl- T8 34.60 34.80 35.00 35.20 m/z 265.10 31.53%| 5000 91 39 103 51 63 77 27

m/z-> I 1 ' 40r ' 1+4a60l.,—pul80pa 100 20 nr । , 1 I 1 1 1 1 | 1 1 1 1 | । 1 । 1 | i ri I | I i | | | i | | | | । | i i p i 120 140 160 180 200 220 240 260 ................. ......... 34.60 34.80 35.00 35.20

9771.D 050102.M Tue May 07 15:44:23 2002 Page 19

NYC-WTC_000043916

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NYC-WTC_000043916Source: NYC Law Department, mirrored locally

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