GCMS calibration results, sample AE06048, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAY02 02\CAL8 0.D Vial: 2 Acq On 2 May 2002 3:42 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 3 8:03 2002 Quant Results File: GCMS0501.RES

Quant Method C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title 209 625/TCLP calibration table Last Update Wed May 01 10:40:31 2002 Response via Initial Calibration DataAcq Meth GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.20 152 472067 40.00 ug/1 -0.01 10) Naphthalene-d8 15.84 136 1719381 40.00 ug/1 -0.01 17) Acenaphthene-diO 21.15 164 914444 40.00 ug/1 0.00 30) Phenanthrene-diO 25.59 188 1319300 40.00 ug/1 0.00 38) Chrysene-dl2 33.65 240 897359 40.00 ug/1 -0.01 44) Perylene-dl2 37.89 264 568554 40.00 ug/1 0.00

System Monitoring Compounds 2 8) TCMX 23.29 209 43422 9.75 ug/L 0.00 Spiked Amount 10.000 Recovery = 97.50%

Target Compounds So/0% Qvalue 2) N-nitroso-dimethyl amine 5.85 74 936668 72.57 ug/1 99 3) bis(2-Chloroethyl)ether 11.60 93 1235583 73.80 ug/1 97 4) 1,3-Dichlorobenzene 12.10 146 1164984 79.19 ug/1 99 5) 1,4-Dichlorobenzene 12.25 146 1268342 78.89 ug/1 99 6) 1,2-Dichlorobenzene 12.76 146 1104551 79.24 ug/1 99 7) 2,21 -oxybis(1-Chloropropan 13.08 45 2427933 70.16 ug/1 99 8) N-Nitroso-di-n-propylamine 13.48 70 908160 72.38 ug/1 99 9) Hexachloroethane 13.61 117 455595 75.44 ug/1 96 11) Nitrobenzene 13.89 77 1066426 68.10 ug/1 99 12) Isophorone 14.53 82 2257754 74.37 ug/1 99 13) bis(2-Chloroethoxy)methane 15.22 93 1439922 74.73 ug/1 99 14) 1,2,4-Trichlorobenzene 15.73 180 946856 81.30 ug/1 99 15) Naphthalene 15.91 128 2835379 78.76 ug/1 100 16) Hexachlorobutadiene 16.45 225 441434 82.50 ug/1 99 18) Hexachlorocyclopentadiene 18.64 237 350995 75.74 ug/1 99 19) 2-Chloronaphthalene 19.41 162 1601583 79.32 ug/1 98 20) Dimethylphthalate 20.51 163 2015892 78.42 ug/1 100 21) 2,6-Dinitrotoluene 20.73 165 352663 63.15 ug/1 99 22) Acenaphthylene 20.68 152 2876544 79.16 ug/1 100 23) Acenaphthene 21.25 153 1688015 79.18 ug/1 ■ 99 24) 2,4-Dinitrotoluene 21.89 165 379256 63.34 ug/1 96 25) Diethylphthalate 22.64 149 1818447 77.98 ug/1 100 26) 4-Chlorophenyl-phenylether 22.79 204 904399 81.99 ug/1 98 27) Fluorene 22.77 166 1817159 79.97 ug/1 99 29) Azobenzen/ 1,2-Diphenylhyd 23.25 77 2256268 72.03 ug/L 98 31) N-Nitrosodiphenylamine 23.18 168 599321 68.52 ug/1 96 32) 4-Bromophenyl-phenylether 24.25 248 517503 80.75 ug/1 98 33) Hexachlorobenzene 24.69 284 590112 82.44 ug/1 97 34) Phenanthrene 25.66 178 2510691 78.52 ug/1 100

(#) = qualifier out of range (m) = manual integration CAL80.D GCMS0501.M Fri May 03 09:43:34 2002 Page 1

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