Liquid-liquid extraction log sheet, May 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0302\CAL20.D Vial: 2 Acq On 3 May 2002 2:58 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 6 9:31 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 521259 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 1905664 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.13 164 1007460 40.00 ug/1 -0.02 30) Phenanthrene-diO 25.58 188 1418407 40.00 ug/1 -0.02 38) Chrysene-dl2 33.64 240 941614 40.00 ug/1 -0.02 44) Perylene-dl2 37.88 264 595853 40.00 ug/1 0.00

System Monitoring Compounds 28) TCMX 23.28 209 53531 10.91 ug/L -0.01 Spiked Amount 10.000 Recovery = 109.10%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.84 74 279819 19.63 ug/1 99 3) bis(2-Chloroethyl)ether 11.59 93 362048 19.58 ug/1 99 4) 1,3-Dichlorobenzene 12.09 146 338309 20.83 ug/1 99 5) 1,4-Dichlorobenzene 12.24 146 371752 20.94 ug/1 100 6) 1,2-Dichlorobenzene 12.75 146 322956 20.98 ug/1 100 7) 2,2'-oxybis(1-Chloropropan 13.07 45 715600 18.73 ug/1 99 8) N-Nitroso-di-n-propylamine 13.45 70 263423 19.01 ug/1 100 9) Hexachloroethane 13.60 117 132940 19.94 ug/1 97 11) Nitrobenzene 13.88 77 301067 17.35 ug/1 100 12) Isophorone 14.52 82 654125 19.44 ug/1 99 13) bis(2-Chloroethoxy)methane 15.21 93 419305 19.64 ug/1 100 14) 1,2,4-Trichlorobenzene 15.72 180 272606 21.12 ug/1 100 15) Naphthalene 15.88 128 834540 20.92 ug/1 99 16) Hexachlorobutadiene 16.43 225 124825 21.05 ug/1 99 18) Hexachlorocyclopentadiene 18.62 237 91357 17.89 ug/1 97 19) 2-Chloronaphthalene 19.39 162 458698 20.62 ug/1 97 20) Dimethylphthalate 20.48 163 578688 20.43 ug/1 100 21) 2,6-Dinitrotoluene 20.70 165 90486 14.71 ug/1 98 22) Ac enapht hylene 20.67 152 840045 20.98 ug/1 100 2 3) Acenaphthene 21.23 153 494724 21.06 ug/1 99 24) 2,4-Dinitrotoluene 21.87 165 86955 13.18 ug/1 97 25) Diethylphthalate 22.62 149 521634 20.31 ug/1 100 26) 4-Chlorophenyl-phenylether 22.77 204 258427 21.27 ug/1 98 27) Fluorene 22.75 166 527963 21.09 ug/1 99 29) Azobenzen/ 1,2-Diphenylhyd 23.23 77 662941 19.21 ug/L 99 31) N-Nitrosodiphenylamine 23.16 168 194756 20.71 ug/1 99 32) 4-Bromophenyl-phenylether 24.24 248 143034 20.76 ug/1 98 33) Hexachlorobenzene 24.67 284 165444 21.50 ug/1 98 34) Phenanthrene 25.64 178 718149 20.89 ug/1 100

(#) = qualifier out of range (m) = manual integration CAL20.D GCMS0501.M Mon May 06 13:34:23 2002 Page 1

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