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GCMS quantitative results for sample AE07633, April 2002

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Gas chromatography-mass spectrometry report for sample AE07633 analyzed April 3-10, 2002, showing detected levels of semivolatile organic compounds.

NYC-WTC_000040174–000040177

Folder label: “GCMS X 4/3/02 A 4/10/02

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NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed)

Data File : C:\MSDCHEM\l\DATA\020410\0410C3.D Vial: 2 Acq On : 10 Apr 2002 11:07 am Operator: Nefliu Sample : ccv Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 10 12:10:26 2002 Quant Results File: SCANAPR0902 .R

Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Tue Apr 09 14:51:40 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

34) Phenanthrene 31.01 178 11596376 25.62 ug/1 99 35) Anthracene 31.24 178 11331593 25.81 ug/1 100 36) Di-n-butylphthalate 33.99 149 12368144 27.13 ug/1 99 37) Fluoranthene 35.24 202 12233134 26.33 ug/1 99 40) Pyrene 35.85 202 12648271 26.66 ug/1 99 41) Buthylbenzylphthalate 38.10 149 4750881 26.89 ug/1 99 42) Benz(a)anthracene 39.09 228 9714898 26.37 ug/1 100 43) Chrysene 39.17 228 9410341 26.05 ug/1 100 44) Bis(2-ethylhexyl)phthalate 39.68 149 5412474m 26.92 ug/1 46) Di-n-Octyl phthalate 41.19 149 6800256m 26.31 ug/1 47) Benzo(b)fluoranthene 41.54 252 6850349 26.18 ug/1 98 48) Benzo(k)fluoranthene 41.60 252 7635880m 25.40 ug/1 49) Benzo(a)pyrene 42.18 252 5918627m 26.82 ug/1 50) Indeno(1,2,3-cd)pyrene 44.36 276 3065779m 24.72 ug/1 51) Dibenz(a,h)anthracene 44.46 278 3120386m 24.73 ug/1 52) Benzo(ghi)perylene 44.90 276 3500648m 26.77 ug/1

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0410C3.D SCANAPR0902.M Thu Apr 11 14:05:39 2002 Page 2

NYC-WTC_0000401 76

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NYC-WTC_000040176Source: NYC Law Department, mirrored locally

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