GCMS analysis results for sample AE06994, April 2002

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d Data File C:\HPCHEM\l\DATA\APR0405\6994.D Vial: 23 Acq On 6 Apr 2002 5:35 pm Operator: Sample gc/ms scan 3/26 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L Peak Number 3 3-Octanol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 15.81 1.80 ug/1 131304 Naphthalene-d8 15.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Octanol 130 C8H180 020296-29-1 38 2 3-Heptanol, 6-methyl- 130 C8H180 018720-66-6 38 3 3-Octanol 130 C8H180 000589-98-0 36 4 Guanidine 59 CH5N3 000113-00-8 32 Abundance Scan 1172 (15.808 min): 6994 D (-) m/z 59.05 100.00% 43 59

5000 83

101 .. 141 15.40 15.60 15.80 16.00 16.20

mlz-> - 4 +51 - 11111111111 +— ----- 70 159 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 1 116 m/ z 43.05 81.34% Abundance #5530: 3-Octanol 59

5000 83 15.40 15.60 15.80 16.00 16.20 31 m/ z 82.95 42.06% 44 101 4 TTTTTTT I I | I 1'1 ! | | I 11 ■ ■ ' ■ । ■ ■ ■ ■ । ■ I 112 T । ■11 ■ ।' ■ ■11111 ■ 111. ■ । > ■. ■ । ' 1111 > c»। m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #5543: 3-Heptanol, 6-methyl- 59

83 ..... 44...... 15.40 15.60 15.80 16.00 16.20 5000 m/ z 56.00 16.41% 27 101 69 | 112 m/z-> 11 1 1 ' 1 r ■ ■11 11 1 1 i'1 20 30 40 50 —P 70 80 60 I 11 1'1 ■ i' ■ ■1 i 11 ‘1 i 1 1 11 r 1 11 1 1 1 1 1 i ’ 1 111 11 90 100 110 120 130 140 150 160 Abundance #5545: 3-Octanol i 1 ■ ■ r i 1 ' 59 15.40 15,60 15.80 16.00 16.20 m/ Z 58.05 15.91% 5000 31 83

42 101

■ i ■ ■' 11 1 TITTTTITITTTTT TTT 112 [ P —T I TT TT I I I —T I TTT TT r TT * r ■ • । ■ i • ■ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 15.40 15.60 15.80 16.00 16.20

6994.D GCMS0408.M Mon Apr 15 14:44:20 2002 Page 3

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