GCMS analysis results for sample AE06760, April 16-19, 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\0416 0 2\LBAO 416.D Vial: 4 4 Acq On : 16 Apr 2002 11:02 am Operator: Bohik Sample : LB 3/21/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Tricyclo[3.3.2.0(3,7)]decan... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

10.26 0.86 ug/L 58548 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tricyclo[3.3.2.0(3,7)]decan-9-one 150 C10H14O 000000-00-0 14 2 Tricyclo[3.3.1.1(3,7)]decanone (... 150 C10H14O 000700-58-3 10 3 2-Adamantanone 150 C1OH140 000700-58-3 10 4 Benzo[b]thiophene-2-ol 150 C8H6OS 000000-00-0 9 Abundance Scan 1222 (10.259 min): LBA0416.D (-) m/z 150.00 100.00% 150

5000 115 76 52

I JR 10.00 10.20 10.40 10.60 40 m/z 152.00 51.97% m/z-> Abundance 0 TITI 20 30 40 50 60 70 80 90 100 110 120 130 140 150 #47200: Tricyclo[3.3.2.0(3.7)]decan-9one p-rTTp-rrrp-r TTTT n 107 150

5000 41 67 79

95

121 "m/i 10.00 10.20 10.40 10.60 m/z 115.10 40.29% 27 53 — Of TT Tr — 4— ‘I‘

Ml m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #46990: Tricyclo[3.3.1.1(3,7)]decanone (CAS) S$ Adamantane... 150

' I ' ' 79 10.00 10.20 10.40 10.60 5000 m/z 76.10 29.02%

41 93 104 117 54 67 132 III 1 THp

i 0- TIT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #46989:2-Adamantanone T-T-p-r-r-r-p-r 150 10.00 10.20 10.40 10.60 m/z 78.10 24.39% 79 5000

41

0 ' i'''' r ‘' r 54 lll 67 93 104 17 132 '11" " i' " I" " i " " i1" ' i " ■" i' Hi m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 10.00 10.20 10.40 10.60

BA0416.D 5080402BBC.M Thu Apr 18 13:01:10 2002 Page 3

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