GCMS analysis results for sample AE06590, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\041502\6590.D Vial: 14 Acq On : 15 Apr 2002 8:45 pm Operator: Bohik Sample : SAMPLE 6590 3/20/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 5 8gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 3-Pentanol, 2,4-dimethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.42 10.36 ug/L 765057 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 33 2 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H14O 000994-05-8 33 3 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 33 4 Pentanol, 5-amino- 103 C5H13NO 002508-29-4 9 Abundance Scan 399 (5.423 min): 6590.D (-) m/z 73.10 100.00% 73

5000

43 I ' ' ■ 1 i ' ' ‘ 11111111 5.00 5.20 5.40 5.60 5.80 87 103 m/z 43.10 22.76% 0 ................... . ................ 'J, I— i ■' • • i1 ' ■' i'' 1 ' i ' '1 11' 1 ti/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #17063: 3-Pentanol, 2,4-dimethyl- 73

5000 55 5.00 5.20 5.40 5.60 5.80 43 m/z 45.10 9.48% 27 15 83 Hr ITII 101 115 m/z—> 01 mP 10 20 30 40 50 60 70 80 . 11 । ।,,,. । , ,.. ।, 90 100 110 120 Abundance #9702: Butane, 2-methoxy-2-methyl- $S Ether, methyl tert-p... 73 _- 5.00 5.20 5.40 5.60 5.80 m/z 41.10 8.34% 5000

43 55 87 29 0! - -l > I r TIPTr 1 80 ■ • ■ i ■'111 ■ ■■■i'■■■i ■ ■ ■ ■ i ■'

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #17065: 3-Pentanol, 2,4-dimethyl- 73 5.00 5.20 5.40 5.60 5.80 m/z 71.10 6.90%

5000 55

43 27

rn/z-> 0 ‘ ■ i ■ ■ ■' i ■ ■ 10 20 4444 165.1 83 91 98 105 114 11 30 40 50 60 70 80 90 I' TTIII 100 110 120 i ■ ■ ' 1 i ' ' 1 5.00 5.20 5.40 5.60 5.80

5590.D 5080402BBC.M Wed Apr 17 18:04:07 2002 Page 3

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