GCMS analysis results for sample AE08949, April 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C:\MSDCHEM\1\DATA\042202\8949.D Vial: 11 Acq On : 22 Apr 2002 7:21 pm Operator: Bohik Sample : SAMPLE 8949 4/15/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L Peak Number 1 2-Pentanone, 4-hydroxy-4-me. .. Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.49 16.19 ug/L 1133950 1,4-Dichlorobenzene-d4 9.41 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 83 2 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 83 3 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 83 4 2-Pentanone, 4-hydroxy-4-methyl-— 116 C6H12O2 000123-42-2 74 Abundance Scan 411 (5.494 mln): 8949.D (-) m/z 43.10 100.00% 43 59

5000

101 5.20 5.40 5.60 5.80 83 m/z 59.10 70.24% miz-> Ot T t ‘ I ‘ 10 20 30 40 50 60 70 80 90 100 110 120 130 * 11,1 i •■ ■ ■ i

Abundance #16593:2-Pentanone, 4-hydroxy-4-methyl- (CAS) $$ Diaceton... 43

5000 i ■ • ■ * i T TTTrr 59 5.20 5.40 5.60 5.80 m/z 58.10 27.96% 31 101 Of " i" 11 n , mln 51 — 70 1 i1" • i • 83 • i ■ mHmmmmmmmm miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130. Abundance #16600: 2-Pentanone, 4-hydroxy-4-methyl- 43 ■i ■ J i t । r ft T TTTT 5.20 5.40 5.60 5.80 5000 m/z 101.10 17.15% 59

15 101 31

n/z-> 01 Tprrt -+++514 TT 1111.11.. i, । i ■ 83 • i , I"

Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 #16606:2-Pentanone, 4-hydroxy-4-methyl- (CAS) $$ Diaceton... .. । ■... ।, I m 43 5.20 5.40 5.60 5.80 m/z41.10 6.27%

5000 59

0 • i ■ ■ “ i■ -4114 . 83 . ।।।11<।।।।k. । j 101 । 133 -444 m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.20 5.40 5.60 5.80

8949.D 5080402BBC.M Thu Apr 25 14:40:05 2002 Page 3

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