GCMS analysis results for sample AE08953, April 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\042202\8953.D Vial: 15 Acq On : 22 Apr 2002 10:38 pm Operator: Bohik Sample : SAMPLE 8953 4/15/02 Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: LSCINT.P.

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.50 16.16 ug/L 997613 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 83 2 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H12O2 000123-42-2 72 3 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 72 4 2-Pentanone, 4-hydroxy-4-methyl-... 116 C6H1202 000123-42-2 72 Abundance Scan 412 (5.500 min): 8953.D (-) m/z 43.10 100.00% 43 59

5000

101 8.B.B । i l TT"|r" *114*1189 5.20 5.40 5.60 5.80 83 miz-> 0+ mmml +11 TIT 10 20 30 40 50 60 70 80 90 100 110 120 130 PHP " i • • • • r • “ i' m/z 59.10 69.43%

Abundance #16606:2-Pentanone, 4-hydroxy-4-methyl- (CAS) $$ Diaceton... 43

5000 T-r-p-m-p-r 59 5.20 5.40 5.60 5.80 m/z58.1027.67% 101

miz-> Ot 44514 t 83 TTTpi • r * ■ • i •* “ I * T 133 10 20 30 40 50 60 70 80 90 100 110 120 130 >l“ ■i “I

Abundance #16613:2-Pentanone, 4-hydroxy-4-methyl- (CAS) $$ Diaceton... 43 ■f ■ I' “ 11"1 ■n-p-m-p-r 59 5.20 5.40 5.60 5.80 5000 rn/z 101.10 18.27% 101

m/z-> Of I “ ' ’ I 10 20 T M.ull 69... 33.... | 30 40 50 60 70 80 90 100 110 120 130 ......... T’ Abundance #16600:2-Pentanone, 4-hydroxy-4-methyl- 43 5.20 5.40 5.60 5.80 m/z56.10 6.24%

5000 59

15 101 31 O' ----+-+-451+ r..... 83.... • ■ i" ■ ■ i • ■ ■ • i ■ -n-p-r-n-p ail m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.20 5.40 5.60 5.80

8953.D 5080402BBC.M Fri Apr 26 12:00:04 2002 Page 3

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