GCMS analysis results for sample AE06762, April 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\041602\6762.D vial: 10 Acq On : 16 Apr 2002 4:02 pm Operator: Bohik Sample : SAMPLE 6762 3/21/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Benzene-1,2,3,4-d4-, 5,6-di... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

10.26 0.81 ug/L 56570 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Benzene-1,2,3,4-d4-, 5,6-dichlor... 150 C6D4C12 002199-69-1 91 2 1,4-Dichlorobenzene-d4 150 C6D4C12 003855-82-1 91 3 1,2-Dichlorobenzene-d4 $$ Benzen... 150 C6D4C12 002199-69-1 91 4 1,4-Dichlorobenzene-d4 150 C6D4C12 003855-82-1 64 Abundance Scan 1222 (10.259 min): 6762.D (“-) m/z 150.00 100.00% 150

5000 115 52 78

87 10.00 10.20 10.40 10.60 JU 40 0 t..j.... ।■ 1111 >11> ■ ।.. . . 11 . . . 11 11111 ITIj ! 1 111 III 111 11 I II0‘T m/z 152.00 72.39%

"w m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130140 150 160 Abundance #41699: Benzene-1,2,3,4-d4-, 5,6-dichloro- $$ 1,2-Dichloro... 150

115 5000 52 78 10.00 10.20 10.40 10.60 m/z 115.10 48.79%

12 - 0 TIIIT 38 28 I I 63 | 87 hr AlPP+ T 1 124 J tt/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #41701: 1,4-Dich!orobenzene-d4 150

T-r-p-r 10.00 10.20 10.40 10.60 5000 115 m/z 78.05 40.19%

52 78

m/z-> 01 +12.28..4044162. - 99 87 | 124 10 20 30 40 50 60 70 80 90 100110 120130140150160 yanbl Abundance #41700: 1,2-Dichlorobenzene-d4 $$ Benzene-1,2,3,4-d4-, 5,6... 150 10.00 10.20 10.40 10.60 m/z 52.10 40.06%

5000 115 78

m/z—> 0 i ■" ‘ i' ’" i 40 52

........... 1 "I"' 'I"1 I 87 I " 1' I " " I " 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 4 1111' i MMuni i-p-r 10.00 10.20 10.40 10.60

>762.D 5080402BBC.M Thu Apr 18 16:08:01 2002 Page 3

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