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GCMS analysis results for sample AE06796, April 2002

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Laboratory report documenting GCMS analysis of environmental sample AE06796 conducted on April 19, 2002.

NYC-WTC_000040011–000040019

Folder label: “GCMS X 3/21/02 A 4/16/02

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Scanned page image, NYC-WTC_000040018
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\041602\6796.D Vial: 14 Acq On : 16 Apr 2002 7:21 pm Operator: Bohik * Sample : SAMPLE 6796 3/21/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Butane, 2-methoxy-2-methyl-... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 5.44 5.30 ug/L 399390 1,4-Dichlorobenzene-d4 9.41 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 38 2 3-Pentanol, 3-methyl-, 102 C6H140 000077-74-7 36 3 N-Ethylformamide $$ N-Formylethy. . . 73 C3H7NO 000627-45-2 9 4 1,3-Dioxolane, 2-heptyl- 172 C10H20O2 004359-57-3 9 Abundance Scan 401 (5.435 min): 6796.D (-) m/z 73.10 100.00% 73

5000

43 ........................................ — 5.00 5.20 5.40 5.60 5.80 87 0 1 i ' ' ' ■ i ' ' 1 ■ i ' 1149 55,.... .1, — ' ■ ■ i • 1 ' । | ' ' ' 'i । ■ I 103 ' i ’ ■ ■ ■ i ■ ' ' ■ i ' ■ ' 1 i ' m/z 43.10 22.14% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9702: Butane, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73

5000 TTMAAr 5.00 5.20 5.40 5.60 5.80 43 55 m/z 45.10 10.66% 87 29

m/z-> _5 7 -8--PP 0- ■ ■ । ’ 1 1 1 I 1 1 TT—rru]iir i । TT 10 20 30 40 50 60 70 80 90 100 110 Abundance #9663: 3-Pentanol, 3-methyl- 73

■ I ■ ' ' ' i ' ' 5.00 5.20 5.40 5.60 5.80 5000 m/z 41.10 3.82%

55 1 45 87 a ••i• 1i•■ 15 _ 1139 67,. ur ' 11 TTBTTt 1 1 1 1 111,1 1 1 ' 1 1 1 1 1 ' 1 1 ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 5.00 5.20 5.40 5.60 5.80 73 m/z 71.10 8.21%

5000 44 58

18

m/z-> 0 1 ' i ' 10 L TIt 20 30 L . 3811 40 .50,, , , T-r-m i । . . . . । . . . , । . , . . । . . . . । . 60 70 80 90 100 110 —.......... — 5.00 5.20 5.40 5.60 5.80

5796.D 5080402BBC.M Thu Apr 18 17:56:19 2002 Page 3

NYC-WTC_000040018

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NYC-WTC_000040018Source: NYC Law Department, mirrored locally

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