GCMS analysis results for sample AE06631, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\041502\6631.D Vial: 16 Acq On : 15 Apr 2002 10:23 pm Operator: Bohik Sample : SAMPLE 6631 3/20/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Neopentyl amine Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.42 11.96 ug/L 858864 1,4-Dichlorobenzene-d4 9.41

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

l Neopentyl amine 87 C5H13N 000000-00-0 9 2 N-Ethylformamide $$ N-Formylethy. . . 73 C3H7NO 000627-45-2 9 3 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 9 4 Propane, 2-methoxy-2-methyl- (CA... 88 C5H120 _______ 001634-04-4 9 Abundance Scan 399 (5.424 min): 6631 .D (-) m/z 73.10 100.00% 73

5000

43 5.00 5.20 5.40 5.60 5.80 ........ 87............103 m/z 43.10 22.85% 0- ■ l ■ ■ 1 ■ I . ' > । | । i i TII’u । । ri.... . । । TIIr m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #4423: Neopentyl amine 33

5000 5.00 5.20 5.40 5.60 5.80 41 m/z 45.10 8.71% 71 19 87 1 I 65 .81 J.................... 0 ■ ■ i • ■ • ■ । • TTrri m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 73 -TP 5.00 5.20 5.40 5.60 5.80 5000 m/z 41.15 7.33%

44 58

18 • ' I — 0- 3811—— i ■ 1 ' ■ i ' 1 1 ■ । 1 ' 1 . । . . . . । . . . . । . m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #4816: Silane, tetramethyl- (CAS) $$ Tetramethylsilane $$ ... 73 A-AA-A 5.00 5.20 5.40 5.60 5.80 m/z 71.10 7.10%

5000

43 29 59 0 15 TTUOBTTT —l.... hl, —+ 88 ■ ■ i • ■ ■ I । • ■ ■ ■ । ■ i • T‘ ■ ■ i ■ ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 5.00 5.20 5.40 5.60 5.80

6631.D 5080402BBC.M Wed Apr 17 18:24:04 2002 Page 3

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