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GCMS calibration analysis, sample AE06267, March 2002

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GCMS calibration results for sample AE06267 showing quantified organic compounds including nitrosamines and chlorinated solvents.

NYC-WTC_000039213–000039216

Folder label: “GCMS X 3/15/02 A 3/16/02

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NYC 9/11 Public Portal Document

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User: Vinci, David L Westchester Dept, of Labs & Research Date: 03/22/2002 Time: 17:43:43

Sample: AE06267 Analysis: $C1GCMS CALI GCMS Units: ug Started: 3/20/02 11:24 Ended: 3/20/02 11:24 Analyst: MF Result source: manual entry Page: 1

Component Name Viol Result Qualifier MDL 1 n-Nitrosodimethylamine 40.34 2.0 2 bis(2-Chloroethyl)ether 36.95 2.0 “ 3 1,3-Dichlorobenzene 37.51 2.0 4 1,4-Dichlorobenzene 37.49 2.0 15 1,2-Dichlorobenzene 37.62 2.0 16 2,2-oxybis(1-Chloropropane) 37.90 2.0 7 " n-Nitrosodi-n-propylamine 40.02 2.0 __87 Hexachloroethane 39.17 2.0 10 Nitrobenzene 38.34 2.0 11 Isophorone 38.37 2.0 bis(2-Chloroethoxy)methane 38.03 2.0 13 1,2,4-T richlorobenzene 12 38.20 2.0 14 Naphthalene 37.51 2.0 Hexa chlorobutadiene 39.35 2.0 15 2-Chloronaphthalene 38.99 2.0 16 Dimethylphthalate 39.68 2.0 17 2,6-Dinitrotoluene 39.69 2.0 18 Acenaphthylene 38.38 2.0 19 Acenaphthene 38.55 2.0 20 2,4-Dinitrotoluene 40.59 2.0 21 Diethylphthalate 39.52 2.0 22 . 4-Chlorophenylphenylether 38.79 2.0 ' 23 Fluorene 38.06 2.0 24 Azobenzene/1,2-Diphenylhydraz 38.53 2.0 “25... n-Nitrosodiphenylamine 38.34 2.0 26 4-Bromophenylphenylether 38.72 2.0 27 Hexa chlorobenzene 37.99 2.0 28 Phenanthrene 37.66 2.0 29 Anthracene 37.52 2.0 ”30" D i-n-buty l phthalate 38.56 2.0 31 Fluoranthene 38.63 2.0 32 Pyrene 35.79 2.0 '33 Butylbenzylphthalate 37.09 2.0 34 Benzo(a)anthracene 38.36 2.0 35 bis (2-Ethyl hexyl )phthalate 36.78 2.0 “36“' Chrysene 37.98 2.0 37 Di-n-octylphthalate 37.28 2.0 38 Benzo(b)fluoranthene 39.08 2.0 39 Benzo(k)fluoranthene 38.46 2.0 40 Benzo(a)pyrene 38.82 2.0 41 Indeno(1,2,3-cd)pyrene 39.22 2.0 42 43 Dibenz(a,h)anthracene 39.56 2.0 Benzo(g,h,i)perylene 39.45 2.0

NYC-WTC_000039213

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