GCMS calibration results for sample AD28860, Dec 13 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC0601\CAL25.D Vial: 2 Acq On 6 Dec 2001 12:06 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 6 14:58 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

29) 2,4,5-Trichlorophenol 18.46 196 877184 25.27 ug/1 99 30) 2-Chloronaphthalene 18.83 162 2576054 24.60 ug/1 99 31) Dimethylphthalate 19.94 163 2937745 24.08 ug/1 100 32) 2,6-Dinitrotoluene 20.15 165 705833 24.48 ug/1 # 65 3 3) Acenaphthylene 20.09 152 3626557 24.64 ug/1 100 34) Acenaphthene 20.65 153 2579959 24.51 ug/1 99 35) 2,4-Dinitrophenol 20.86 184 218599 19.07 ug/1 # 92 36) 4-Nitrophenol 21.14 65 341105 28.45 ug/1 96 37) 2,4-Dinitrotoluene 21.32 165 896302 24.45 ug/1 92 38) Diethylphthalate 22.08 149 2795166 24.76 ug/1 99 39) 4-Chlorophenyl-phenylether 22.20 204 1247841 25.32 ug/1 99 40) Fluorene 22.17 166 2718807 25.17 ug/1 98 41) Azobenzen/ 1,2-Diphenylhyd 22.67 77 3036034 26.03 ug/L 97 43) 4,6-Dinitro-2-methylphenol 22.53 198 410097 21.69 ug/1 94 44) N-Nitrosodiphenylamine 22.61 168 1170487 24.67 ug/1 95 45) 4-Bromophenyl-phenylether 23.66 248 677698 25.78 ug/1 99 46) Hexachlorobenzene 24.08 284 754163 26.09 ug/1 97 4 7) Pentachlorophenol 24.64 266 365163 26.70 ug/1 99 4 8) Phenanthrene 25.05 178 3540997 25.02 ug/1 99 49) Anthracene 25.19 178 3507766 24.86 ug/1 100 50) Di-n-butylphthalate 26.99 149 4752620 25.23 ug/1 100 51) Fluoranthene 28.67 202 3481920 25.48 ug/1 99 54) Pyrene 29.33 202 3599069 23.30 ug/1 99 55) Butylbenzylphthalate 31.50 149 1898033 23.53 ug/1 95 56) Benzo(a)anthracene 32.97 228 2624004 24.61 ug/1 99 57) Bis(2-ethylhexyl)phthalate 33.29 149 2689187 24.67 ug/1 99 58) Chrysene 33.10 228 2537482 24.27 ug/1 99 60) Di-n-Octylphthalate 35.04 149 4176918 23.15 ug/1 # 97 61) Benzo(b)fluoranthene 36.05 252 2553684 25.00 ug/1 99 62) Benzo(k)fluoranthene 36.11 252 2547724 24.30 ug/1 99 6 3) Benzo(a)pyrene 36.94 252 2155552 24.27 ug/1 99 64) Indeno(1,2,3-cd)pyrene 40.79 276 2234006 25.16 ug/1 99 65) Dibenz(a,h)anthracene 40.86 278 1735359 24.96 ug/1 97 66) Benzo(g,h,i)perylene 41.89 276 1941593 25.59 ug/1 94

(#) = qualifier out of range (m) = manual integration CAL25.D GCMS1126.M Wed Dec 12 11:30:47 2001 Page 2

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