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GCMS analysis results for sample AE02147, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02147 conducted on March 21, 2002, showing surrogate compound data.

NYC-WTC_000038982–000038990

Folder label: “GCMS X 3/8/02 A 3/19/02

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NYC 9/11 Public Portal Document

Library Search Compound Report i • Data File : C:\MSDCHEM\l\DATA\031802\2147.D Vial: 25 Acq On : 19 Mar 2002 9:48 pm Operator: McLean Sample : GC/MS SCAN 3/8 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.06 0.50 ug/L 200694 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 3 Benzeneacetic acid, .alpha.,3,4-... 472 C20H40O5Si4 037148-65-5 43 4 N-(Trifluoracetyl)-0,0',0'‘-tris... 495 C20H36F3NO4S13 054135-51-2 43 Abundance Scan 990 (12.056 min): 2147.D (-) m/z 73.10 100.00% 73

5000 267 355

11.80 12.00 12.20 12.40 0- 45 I, I 154 11,27 323 1 m/z 267.00 47.01% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 ----------- 11.80 12.00 12.20 12.40 355 m/z 355.10 39.99% 45 ■I l 103 133 165 193 223 ! 293 323 |(......... 01 TTPTTTTTT m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

- ... , , , , 355 11.80 12.00 12.20 12.40 267 m/z 356.10 13.81% 5000

45 207 323 0- ' 1 i ' ’ 1 1 i ' ' 1 ■ i 1 1 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #361625: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... 73 11.80 12.00 12.20 12.40 m/z 268.10 9.52%

5000 355

147 47 105 — 193 237 267295 325 :384 429457 0 1 1IT ' TTATe I 11 1 ' 1 1 1 * 1 I -l r > ■ i ■ • > • i ■ m/z—> 50 100 150 200 250 300 350 400 450 11.80 12.00 12.20 12.40

2147.D 5080302.M Wed Mar 20 02:21:44 2002 Page 3

NYC-WTC_000038989

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NYC-WTC_000038989Source: NYC Law Department, mirrored locally

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