NYC-WTC_000038580
Gas chromatography-mass spectrometry analysis report for environmental sample AE04035 dated March 29, 2002.
Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Document / 16 pages
GCMS unknowns report for sample AE02460, March 2002
Machine-extracted title · confidence 90%Laboratory report detailing analysis of unknown compounds and surrogate recovery for sample AE02460.
NYC-WTC_000038801–000038816Folder label: “GCMS X 3/4/02 A 3/20/02”
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OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Llbrary searcn compound Keporc
Data File : C:\HPCHEM\1\DATA\MAR1902\2460.D Vial: 19 Acq On : 20 Mar 2002 10:44 pm Operator: Sample : gc/ms scan 3/4 fb Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
38.86 1.77 ug/1 190312 Perylene-dl2 37.97
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethy1-3,3-bis (t 444 C13H40O5Si6 038147-00-1 37 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 32 3 Trisiloxane, 1,1,1,5,5,5- hexamethyl 384 C12H3604Si5 003555-47-3 12 4 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 10 Abundance 73 Scan 3683 (38.860 min): 2460.D ( ) m/z 73.00 100.00%
147 5000 221 281 355 429 38.60 38.80 39.00 39.20 45 ■ ■'i ■ ' 117 — 193, , 2534 I 327 , — 401 TIT 14 — .1...... m/z 147.00 60.20% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiioxy)t 73 147 5000 267 355 429 38.60 38.80 39.00 39.20 207 m/z _/ 221.0 45 1 ' 1 i 1 r 1 ' i ' ' ' ' I ' 1 1 1 I ' ' 1 1 I ' 1 m/z-__ 50_ 100 150 200 250 300 350 400 450 500 550 Abundance 73 ----- 38.60 38.80 39.00 39.20 5000 m/ Z 355.0 5.05 30.44% 147
221 281 327 415 519 561 m/z-> 50 100.. 150 200 250 300 350 400 450 500 550 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet Ai • 1 I t ' « 73 38.60 38.80 39.00 39.20 147 m/z 281.00 26.98% 5000 281 45 369 117 207 249 , [ 1 ' l 1 ' 1 1 i 1 1 i 1 1 ‘ ■ I ' ■ ■ ■ i ■‘ .............................. / । । । > > .......................... .... । । । । । । i m/z~> 50 100 150 200 250 300 350 400 450 500 550 38.60 38.80 39.00 39.20
2460.D GCMS0308.M Thu Mar 21 14:15:10 2002 Page 5
NYC-WTC_000038812
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NYC-WTC_000038812Source: NYC Law Department, mirrored locally
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