GCMS analysis results for sample AE04035, Mar 2002

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Data File : C:\HPCHEM\1\DATA\MAR2202\4035.D Vial: 41 Acq On : 24 Mar 2002 9:33 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L

Peak Number 5 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

40.62 1.17 ug/1 106667 Perylene-dl2 37.97

Hit# of 5 Tentative I MW Mol Form' CAS# Qual

1 Trisiloxane, 1,1,1,5>/5,5-hexamethyl 384 C12H3604Si5 003555-47-3 27 2 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 25 3 2,6-Dimethyl-3,4-bis (trimethylsilyl 311 C15H29NO2Si2 000000-00-0 22 4 l,l,l,5,7,7,7-He^tamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 12 Abundance Scan 3875 (40.616 min): 4035.D (-) m/ Z 73.00 100.00% 73 147 221 5000 281 355 429 I’ 1 i 1 ' 1 1 1 1 1

m/z-> 11'1" ।" nT mTT .—191 + 423+— 40. 60 80.100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 H l m/ z 14 7.00 327 , 40.20 40.40 40.60 40.80 41.00 65.24% Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyi-3,3-bisi(trimet 73 147

5000 —A-AAAA--TM 281 40.20 40.40 40.60 40.80 41.00 45 369 m/z 221.0 53.38% I , 117 207 249 TTTTEICTCTT P1" r " ■ i I"111 i"11P H11" " i m/z—>40 6080100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance . 7 . . 147 221 AA-— 40.20 40.40 40.60 40.80 41.00 73 5000 m/z 355.05 25.35% 191 117 279 ‘I‘ErTTCTETEEIIETEIIEIEEEII—Immm/1111111101—umau—0110—mmni m/z-> 40. 60 80 100120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #44359: 2,6-Dimethyl-3,4-bis(trimethylsilyioxymethyl)pyridi I.L‘ 73 221 40.20 40.40 40.60 40.80 41.00

m/z-> 5000

45 | । 147

178 | ( , | 296 ' l" " । " i" " i ‘‘ i " i:1 ‘' i ‘‘' I" TT i r '1 [ ■'' ।'1'111"11"1111"11" " I" " I"111" " 111" I"111 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 m/z 281.00

i 1 1 ■ ‘ i ' 7 25.06%

40.20 40.40 40.60 40.80 41.00

4035.D GCMS0308.M Tue Mar 26 10:48:31 2002 Page 5

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