GCMS quantitation results for sample AE04033, March 2002

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Quantitation report listing response data for deuterated internal standards and surrogates from a March 29, 2002 analysis.

NYC-WTC_000038562–000038570

Folder label: “GCMS X 2/25/02 A 3/23/02”

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NYC 9/11 Public Portal Document DCCLUi wupOuIU ACDOL L L Data File : C:\HPCHEM\l\DATA\MAR2202\4033.D Vial: 39 Acq On : 24 Mar 2002 7:35 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.87 1.22 ug/1 229915 Naphthalene-d8 15.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopenta 1oxane, decamet hyl- 370 C10H3005Si5 000541-02-6 91 2 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H3004Si3 010586-16-0 43 3 3,4-Dihydroxymandelic acid, ethyl e 428 C19H3605Si3 000000-00-0 38 4 Silane, [ [4- [1,2-bis [ (trimethylsily 458 C20H42O4Si4 056114-62-6 37 Abundance Scan 1070 (14.866 min): 4033.D (-) i m/z 73.00 100.00% 73

267 355 5000

....... /....... — 45 103 133 154 123 223 249 323 14.60 14.80 15.00 15.20 TT—Tnpr TTTTg TT ' r 1 m T । । ।। । । । TT j TTTTTTOITTTTTTT 11" " i" " i' । m/z 267.00 50.57% miz-2 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000 267 1 .......... 4.............. 14.60 14.80 15.00 15.20 m/z 355.0,5 50.16% 207 249 , 323 i "10—0—00—0001—000—011000—3—01—23— i " " i1'1 r i"' i" " i T" 1' 11 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance l. - 73

14.60 14.80 15.00 15.20___ 5000 355 m/z 356.05 16.51% 45

133 193 223 281

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #55759: 3,4-Dihydroxymandelic acid, ethyl ester, tri-TMS ...... 4........... 3$5 14.60 14.80 15.00 15.20

73 m/ z 268.00 12.35% 5000

208 251 281 385 413 ...... - ‘' ।' "' ।'" 11'1" i " " i r" ' i " " i" ‘ ’ i"'' i" " r 1" i"1 ‘ 1"1' i" 111" " I n 111111 11111111" |'1 r' |1 m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 i 14.60 14.80 15.00 15.20

4033.D GCMS0308.M Tue Mar 26 10:46:11 2002 Page 1

NYC-WTC_000038569

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