GCMS quantitation results for sample AE04029, March 2002

NYC 9/11 Public Portal Document Library searcn compound Report

Data File : C:\HPCHEM\1\DATA\MAR2202\4029.D Vial: 35 Acq On : 24 Mar 2002 3:38 am Operator: Sample : gc/ms scan 2/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ******************************************************************* ** Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.86 0.81 ug/1 117659 Naphthalene-d8 15.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 90 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 43 3 N- (Trifluoroacetyl) -N,0,0',0' ‘-tetr 553 C22H42F3NO4Si4 000000-00-0 38 4 Benzoic acid. 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 38 Abundance Scan 1069 (14.862 min): 4029.D (-) m/ z 73.00 100.00% 73

5000 267 355 1 I 1 1 T M 45 108 154 193 237, , 325 _ 14.60 14.80 15.00 15.20 i , • • i 1 ■ — T It l' |"i ■ ■ I 1 -r ' ' i m/z 267.00 43.98% m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 1-1/1/1/1/11/1/1/1/1/1/1/1 5000 14.60 14.80 15.001 15.20 m/ z 355.05 40.58% t , 207, -323 m/z->_____ 50___ 100 150 _ 200 250 300 350 400 450 500 550 Abundance aapans ; omsydrokybenry a mamapegikimettyglyit. 73 ...... J /....... 14.60 14.80 15.00 15.20 267 m/z 356.05 5000 179 15.85% 356 45 147 i .......................... 209 237 312 m/z->___ _ 50 100__ 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacety!)-N,O,O ‘,O"-tetrakis(trimethylsi It" 73 14.60 14.80 15.00 15.20 m/ z 268.00 11.21% 355 5000

45 T I I III „ 147 193 267 538 ,.......... 1 ............ miz-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

4029.D GCMS0308.M Tue Mar 26 10:42:59 2002 Page 2

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