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GCMS method 508 scan data for WTC samples, March 2002

Machine-extracted title · confidence 90%

Instrument data file containing chromatographic scans and compound identification for environmental samples analyzed in March 2002.

NYC-WTC_000037884–000037905

Folder label: “GCMS X 2/20/02 A 3/20/02

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Scanned page image, NYC-WTC_000037889
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\3800.D Vial: 10 Acq On : 19 Mar 2002 7:02 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Ethane, 1,1,2,2-tetrachloro... Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T.

7.49 0.63 ug/L 207766 1,4-Dichlorobenzene-d4 9.54

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethane, 1,1,2,2-tetrachloro- (CA... 166 C2H2C14 000079-34-5 97 2 Ethane, 1,1,2,2-tetrachloro- (CA... 166 C2H2C14 000079-34-5 94 3 Ethane, 1,1,2,2-tetrachloro- 166 C2H2C14 000079-34-5 93 4 Ethane, 1,1,2,2-tetrachloro- (CA... 166 C2H2C14 000079-34-5 64 Abundance Scan 487 (7.493 min): 3800.D (-) m/z 83.00 100.00% 83

5000

60 TTIITMTT 95 7.20 7.40 7.60 7.80 133 168

miz-> 0 T ..Il ...mm51 , .......I|l,i........ ........ ||......... 11«• t I’TT i 11«> I p •«11 > 111 20 30 40 50 60 70 80 90 100110120130140150160170180 b 111 m/z 85.00 60.39%

Abundance #66401: Ethane, 1,1,2,2-tetrachloro- (CAS) $$1,1,2,2-Tetr... 83

5000 i ‘ ■11 T T 7.20 7.40 7.60 7.80 m/z 60.00 16.14% 26 35 61 95 It I 47 I -70 rn/z—> 0 mmm TTTT 109,119.131,143.157.166.., 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance #66404: Ethane, 1,1,2,2-tetrachloro- (CAS) $$ 1,1,2,2-Tetr... 83

i ’ > • i T 7.20 7.40 7.60 7.80 5000 m/z 61.00 15.31%

35 61 95 47 |„ 131 168

m/z-> olTTTTT-7 +1081171431554. 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #66399: Ethane, 1,1,2,2-tetrachloro- ‘ ' l ‘ 1 1 • I ' ' ‘ • I " ' 7.20 7.40 7.60 7.80 m/z 94.90 13.11%

5000

26 35 47 60 131 168

miz—> 0. -+.4,70. 20 30 40 50 60 70 80 90 100110120130140150 160170180 7.20 7.40 7.60 7.80 3800.D 5080302.M Thu Mar 21 11:42:12 2002 Page 3

NYC-WTC_000037889

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NYC-WTC_000037889Source: NYC Law Department, mirrored locally

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