GCMS analysis report, sample AE02338, March 22, 2002

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Data File C:\MSDCHEM\l\DATA\030402\2338.D Vial: 10 Acq On 4 Mar 2002 5:38 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Ethane, 1,1,2,2-tetrachloro... Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

7.52 0.41 ug/L 136745 1,4 -Dichlorobenzene-d4 9.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethane, 1,1,2,2-tetrachloro- $$ ... 166 C2H2C14 000079-34-5 93 2 Ethane, 1,1,2,2-tetrachloro- (CA... 166 C2H2C14 000079-34-5 90 3 Ethane, 1,1,2,2-tetrachloro- (CA... 166 C2H2C14 000079-34-5 87 4 Ethane, 1,1,2,2-tetrachloro- (CA... 166 C2H2C14 000079-34-5 83 Abundance Scan 490 (7.520 min): 2338.D (-) m/z 83.00 100.00% $ M

5000

47 60 95 133 168 ■ ■ i • • ■ ■ i • 7.20 7.40 7.60 7.80 A.... 01 .................. l.l 1 1 i ■ ■ ■ ■ i ‘ ■ ■ l 1+ Il.......... Il l. 1 , m/z 85.00 71.02% m/z-> 20 40 60 80 100 120 140 160 180 Abundance #66403: Ethane, 1,1,2,2-tetrachloro- $$ S-Tetrachloroethan... 83

- 5000 7.20 7.40 7.60 7.80 95 m/z 60.00 23.35%

m/z-> 01 123447 20 40 60 k • i • ' 80 ------- 100 120 140 160 131 168

180 Abundance #66404: Ethane, 1,1,2,2-tetrachloro- (CAS) $$ 1,1,2,2-Tetr... 83 i1'111 ITrr r ■ • । ■ ■ ■ ■ । ■ 7.20 7.40 7.60 7.80 5000 m/z 95.00 20.99%

35 61 95 47 I i, 131 168

miz-> Of — ■ ■ 20 — 40 „1,., 60 72,80, .,105117.1, 100 120 143.155 4 . , 140 160 180 Abundance #66401: Ethane, 1,1,2,2-tetrachloro- (CAS) $$ 1,1,2,2-Tetr... 83 »••••! T I ‘ ' I 7.20 7.40 7.60 7.80 m/z 61.00 14.13%

5000

26 61 95 , I., 131 168 11 37 47 0 ----44 72—14. 109119 ih..143 157 ,h "B r । r >“T"i । > i rr 1’T5T T T T m/z-> 20 40 60 80I 100 120 140 160 180 7.20 7.40 7.60 7.80

2338.D 5080302.M Mon Mar 18 08:32:09 2002 Page 3

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