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GCMS analysis report for sample AE02335, March 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010513–000010536

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

• •Data File C:\MSDCHEM\l\DATA\030402\2334.D Vial: 14 Acq On 4 Mar 2002 8:54 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Ethane, 1,1,2,2-tetrachloro... Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

7.52 0.43 ug/L 140022 1,4-Dichlorobenzene-d4 9.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethane, 1,1,2,2-tetrachloro- (CA... 166 C2H2C14 000079-34-5 87 2 Ethane, 1,1,2,2-tetrachloro- (CA... 166 C2H2C14 000079-34-5 87 3 Ethane, 1,1,2,2-tetrachloro- 166 C2H2C14 000079-34-5 81 4 N,N-Dimethyl-2H-pyran-2-iminium ... 159 C7H10C1NO 000000-00-0 53 Abundance Scan 490 (7,520 min): 2334.D (-) m/z 83.00 100.00% 83

5000

61 95 - ,r,

m/z—> 0 " i ■ ■1 ■ r ■ 47 4 ltle 20 30 40 50 60 70 80 90 100110120130140150160170180 7.20 7.40 7.60 7.80 m/z 85.00 62.01%

Abundance #66404: Ethane, 1,1,2,2-tetrachloro- (CAS) $$1,1,2,2-Tetr... 83

5000 A i • 11 ■ I • ■ i ■ • • ■ i T 7.20 7.40 7.60 7.80 35 m/z 95.00 19.82% 61 95 47 131 168 "itt' ■ T"11 p*1 1143 1ITTI’155 ,1 Ih. . ii 70 0 ’ I’TTITWTTTTTTMpit 1108117 »n r1 1. TTTn... ’TT /z-> 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance #66401: Ethane, 1,1,2,2-tetrachloro- (CAS) $$1,1,2,2-Tetr... 83 ■' i ■1 ‘11 ■ ■ ■ i ■ ‘■ i ■ ■ ■ ■ i 7.20 7.40 7.60 7.80 5000 m/z 61.00 17.83%

26 35 61 95 , | 47 0 mm V-r.frJR.r,1,1.1 109,119,141443,157 1ff. m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance #66399: Ethane, 1,1,2,2-tetrachloro- 83 • ■ i ■ ■ • ■ i1 7.20 7.40 7.60 7.80 ■ ‘' ■ • i • ■ ■ ■ i

m/z 60.00 16.09%

5000

26 35 60 96 131 168 47 01 MlHlpmzilmmmmmmlmpmm ’I’ *’1**’*# • • i • ■ ■ ‘ i ■1 /z—> 20 30 40 50 60 70 80 90 100110120130140150160170180 7.20 7.40 7.60 7.80

2334.D 5080302.M Mon Mar 18 08:30:52 2002 Page 3

NYC-WTC_000010520

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NYC-WTC_000010520Source: NYC Law Department, mirrored locally

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