GCMS analysis results, sample AE05301, March 2002

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Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\031602\5301.D Vial: 20 Acq On 17 Mar 2002 2:24 am Operator: McLean Sample 3/9 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.56 2.50 ug/L 733387 1,4-Dichlorobenzene-d4 9.54 / Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 40 2 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 9 3 1,3-DioxolaneZ 2-methyl- (CAS) $... 88 C4H8O2 000497-26-7 9 43-(CYCLOHEX-3 '-EN-YL)PROPANOL $$... 174 C8H14O4 _____ 015745-87-6 9 Abundance / Scan 274 (5.561 min); 5301 .D (-) m/z 73.10 100.00% 7|3

5000

I I 45 5.20 5.40 5.60 5.80 Oi 1 ' ' ‘ ‘ I ' ' ' ' I ' ' ' ' I ' ‘ ' I ' ' ' I 55 I....... 87........ 103 m/z 45.10 12.78% m/z-> 0 10 20 30 40 50 60 70 80 90 100 110 Abundance #4814: Silane, tetramethyl- 73

5000 ' I ' ' ' ' I ' ' ' ' . I I 5.20 5.40 5.60 5.80 m/z 71.10 7.15% 43 29 0 2 ,1 , 36 I ihl_,^,^, .60 -n/z~> 0 10 20 30 40 50 60 70 80 90 100 110 Abundance #4813: Silane, telramethyl- (CAS) SS Tetramethylsiiane SS ... 73

■p" 5.20 5.40 5.60 5.80 ) m/z 69.10 4.79% 5000

45 29 15 Ji III 53 66 I, 88 Oi Tl/Z~> 0__J0_^0__J0_J:0__J0__60__7CL_^^ Abundance #4687: 1,3-Dioxolane, 2-methyl- (CAS) $$ 2-Methyl-1,3-diox... 73 5.20 5.40 5.60 5.80 43 m/z 74.10 4.71%

5000 58

87 0 .... .. ............. A l y m/z~> 0 10 20 30 40 50 60 70 80 90 100 110 5.20 5.40 5.60 5.80

5301.D 5080302.M Wed Mar 20 08:52:29 2002 Page 3

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