Instrument data file containing chromatographic scans and compound identification for environmental samples analyzed in March 2002.
NYC-WTC_000037884–000037905Folder label: “GCMS X 2/20/02 A 3/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
» Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\031902\3800.D Vial: 10 Acq On : 19 Mar 2002 7:02 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L
Peak Number 2 Cyclotetrasiloxane, octamet... Concentration Rank 11
R.T. EstConc Area Relative to ISTD R.T.
8.91 1.08 ug/L 356905 1,4-Dichlorobenzene-d4 9.54
Hit# of 5 Tentative ID MW MolForm CAS# Qual
l Cyclotetrasiloxane, octamethyl- ... 296 C8H24O4Si4 000556-67-291 2 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 $91 3 Cyclotetrasiloxane, octamethyl- ... 296 C8H24O4Si4 000556-67-2 91 4 Cyclotetrasiloxane, octamethyl- ... 296 C8H24O4Si4; 000586-67-2 90 Abundance Scan 643 (8.908 mln): 3800.D (-) m/z 281400 100.00% 281
5000
T T “T I 73 133 193 249 8.60 8.80 9.00 9.20 0 56 | mpmmmmmp 103 163I k I L m/z 282.10 28.84% miz-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #244216: Cyclotetrasiloxane, octamethyl- (CAS) $$ 1,1,3,3,... 281
5000 .. 1... •' I' ‘ ‘ ‘ I ■ ‘ ‘' 1' ‘ ' i' ' I 8.60 8.80 9.00 9.20 m/z 283.00 16.11%
28 45 73 103 133 163 193 d 249 [ L 0--i TITTIT TTppn T TItI T 111 ri^ । Th TDTIT miz-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #244215: Cyclotetrasiloxane, octamethyl- 281
1' 11'1 ■ 11' ■' I' ■ ■' i ■' ■ • 1 8.60 8.80 9.00 9.20 m/z 133.00 9.58% 5000
mtz-> 0 +25,,51,73103..4133.163.144221..248,4.1,299, 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #244214: Cyclotetrasiloxane, octamethyl- $$ Octamethyicycl... 281 TITrr 1111' 1' ‘' 1 8.60 8.80 9.00 9.20 m/z73.10 8.85%
5000
133 207 249 , 15 45 73. .................... - 0 TDmDTem ■' i1 • ■ ■ i ■ ■ ■ • 1 •1111 ■1 ■11 miz—> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 8.60 8.80 9.00 9.20
3800.D 5080302.M Thu Mar 21 11:42:14 2002 Page 4 NYC-WTC_000037890
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000037906
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03801 conducted on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037948
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03804 conducted on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037848
Laboratory report documenting GCMS analysis of a method blank for sample AE03799 to verify analytical system cleanliness.
1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010585
Laboratory analysis report for sample AE02338 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010488
Laboratory analysis report for sample AE02334 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010513
Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010610
Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011347
Laboratory report documenting GCMS blank analysis of environmental sample AE03265 conducted on March 25, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010537
Laboratory analysis report for sample AE02335 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010659
Laboratory report detailing gas chromatography-mass spectrometry analysis of environmental sample AE02381 conducted on March 22, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012129
Laboratory report for GC/MS re-injection of sample 1639 using Method 508 scan on March 20-21, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010558
Laboratory analysis report for sample AE02336 conducted on March 22, 2002, listing unknown compounds and surrogates.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000037819
Department of Environmental Protection site log sheet for the World Trade Center area covering February and March 2002.
Filed in the same folder
NYC-WTC_000037820
Log sheet recording sample preparation details including drip rates and pH for GCMS analysis in March 2002.
Filed in the same folder
NYC-WTC_000037825
Laboratory report listing quantitative concentrations of volatile organic compounds in sample AE00364 analyzed on March 21, 2002.
Filed in the same folder
NYC-WTC_000037829
Reference data report for GCMS analysis of sample AE00364 showing peak identification and response values from March 21, 2002.
Filed in the same folder
NYC-WTC_000037837
Laboratory report documenting GCMS analysis of a method blank for sample AE00364 to verify analytical system cleanliness.
Filed in the same folder