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GCMS surrogate recovery data for PAHs, sample 3731, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS surrogate recovery data for polycyclic aromatic hydrocarbons using EPA Method 508.

NYC-WTC_000037594–000037603

Folder label: “GCMS X 2/19/02 A 3/12/02

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Scanned page image, NYC-WTC_000037600
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search. Compound Report

Data File : C:\MSDCHEM\1\DATA\031202\3731.D Vial: 57 Acq On : 13 Mar 2002 2:46 am Operator: McLean Sample : SAMPLE 3731 2/19/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Humber 2 Carbazole Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

23.28 0.44 ug/L 236085 Phenanthrene -dl0 22.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Carbazole . 167 C12H9N 000086-74-8 93. 2 9h-carbazole (CAS) $$ Carbazole ... 167 C12H9N 000086-74-8 53 3 9H-Carbazole (CAS) $$ Carbazole ... 167 C12H9N 000086-74-8 93 4 9H-Carbazole (CAS) $$ Carbazole ... 167 C12H9N 000086-74-8 93 Abundance Scan 2228 (23.285 min): 3731 .D (-) m/z 167.10 100.00% 167

5000

-----IFF —TFFMAr 1 139 23.00 23.20 23.40 23.60 Of - --+51 *,70144 T . 113I ! al I m/z 166.10 20.76% miz-> 20 40100 120 60 80 140 160 Abundance #69298: Carbazole 167

5000 — 23.00 23.20 23.40 23.60 m/z 139.10 14.74% 139 51 63 75 87 98 115 II I 01 -IIIIIIIF-* miz-> 20 40 60 80 100 120 140 160 Abundance ’: 9H-Carbazole (CAS) $$ Car $$ 9-Azafluorene $... 107

T T T 23.00 23.20 23.40 23.60 m/z 168.10 13.55% 5000

139 14 29 39 51 63 75 89 101 113 —P 1 0! m/z-> 20 40 60 80 100 120 140 160 Abundance #69300:9H-Carbazole (CAS) $$ Carbazole $$ 9-Azafluorene $... 167 T T T 23.0023.20 23.40 23.60 m/z 140.10 10.18%

5000

139 44 63 75 89 113 | 0 11 • ■ i • • • ■ i ■' m/z—> 20 40 60 80 100 120 140 160 23.00 23.20 23.40 23.60

3731.D 5080302.M Fri Mar 15 14:26:59 2002 Page 4

NYC-WTC_000037600

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NYC-WTC_000037600Source: NYC Law Department, mirrored locally

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