GCMS analysis results for sample AE03618, March 29, 2002

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Library Search Compound Report

• Data File : C:\MSDCHEM\1\DATA\031202\3618.D Vial: 55 Acq On : 13 Mar 2002 1:07 am Operator: McLean Sample : FB 2/19/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

12.06 1.78 ug/L 778214 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasi xane, decamethyl- 370 C10H3005Si5 000541-02-6 68 2 N- (Trifluora etyl) -O,O’ ,0"-tris. . . 495 C20H36F3NO4Si3 054135-51-2 43 3 Benzoic acid, 2- [ (trimethylsilyl... 282 C13H2203Si2 003789-35-3 38 4 Butanamide 2,2,3,3,4,4,4-heptaf... 493 C18H26F7N03Si2 055471-01-7 38 Abundance . .... / Scan 990 (12.056 min): 3618.D (-) m/z 73.10 100.00% 73

267 5000 355

1eT T PI T 45 11.80 12.00 12.20 12.40 0- — —125154.123223—+ 11 1 323 +r —IT ■ i • ■ ■ ■ i ■ ■ ‘ ■ I 1 m/z 267.00 50.93% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cycl me, decamethyl- 73

355 267 5000 — ‘ 11.8012'66 12.20 12.40 m/z 355.10 40.20%

45 207 . 0- - । । TT । । ■ ■ ■ frtr 323, I I I j t I TT, I T TI I 1 m/z-> 50 100 150 200 250 300 ".350 400 450 Abundance #367529: N-(Trifluoracety!)-O,0‘,0"-tris(trimethylsilyl)e... 73 355 11.80 12.00 12.20 12.40 5000 m/z 356.10 13.93%

m/z-> 0 4 45

50 110 140 184 221251,281 324 TIITrfifTTffrnTnnguuitgr III 100 150 200 250 480 300 350 400 450 Abundance #227683: Benzoic add, 2-I(trimethylsilyl)oxy]-, trimethyl... 73 267 11.80 12.00 12.20 12.40 m/z 268.00 11.38%

5000

45

m/z—> 0 TIT 50 s1 4994 22———7— 100 150 200 250 300 350 400 450 T> 11.8012'66 12.20 12.40

3618.D 5060302.M Fri Mar 15 14:26:46 2002 Page 3

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