Quality reviewed GCMS calibration data listing surrogate compounds and retention times from December 14, 2001.
NYC-WTC_000036729–000036751Folder label: “GCMS X 12/7/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\DEC1301\29522.D Vial: 21 Acq On : 14 Dec 2001 4:25 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 27 15:06 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 1298761 20.00 ug/1 -0.03 10) Naphthalene-d8 . 15.28 136 4964067 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 2488123 20.00 ug/1 -0.02 29) Phenanthrene-dlO 24.98 188 3678540 20.00 ug/1 -0.01 38) Chrysene-dl2 33.02 240 1979297 20.00 ug/1 -0.01 44) Perylene-dl2 37.10 264 1616202 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.05 235 182201 3.42 ug/mL -0.02 Spiked Amount 5,000 Recovery = 68.40%
Target Compounds ’ Q! Qvalue 2) N-nitroso-dimethyl amine 5.30 74 182 N.D. 3) bis(2-Chloroethyl )ether 10.99 93 703 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D, 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. . 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.35 77 313 N.D. 12) Isophorone 14.08 82 882 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 3257 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.17 163 1227 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 20.57 153 261 N.D. 24) 2,4-Dinitrotoluene 21.27 165 207 N.D. 25) Diethylphthalate 22.06 149 2138 N.D. 26) 4-Chlorophenyl-phenylether 22.39 204 703 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 22.72 77 2821 N.D.
(#) = qualifier out of range (m) = manual integration 29522.D GCMS1126.M Thu Dec 27 15:21:57 2001 Page 1
NYC-WTC_000036729
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1 shared non-person entities · 1 shared topics · similarity 0.984
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