GCMS analysis results for sample AD29734, Jan 2002

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GCMS analysis report for sample AD29734 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036874–000036887

Folder label: “GCMS X 12/7/01 A 1/2/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1301\29734.D Vial: 20 Acq On : 14 Dec 2001 3:26 am Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 27 15:05 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 1246270 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 4730869 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 2310727 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.97 188 3331866 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 2074491 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 1357559 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.05 235 125235 2.6°g/mL -0:02 Spiked Amount 5.000 Recovery £ 52.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.16 74 577 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 . N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.58 77 178 N.D. 12) Isophorone 14.07 82 100 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 2241 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 19.99 163 210 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.16 165 495 N.D. 25) Diethylphthalate 22.07 149 1776 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 23.07 77 276 N.D.

(#) = qualifier out of range (m) = manual integration 29734.D GCMS1126.M Thu Dec 27 15:21:19 2001 Page 1

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