Laboratory commentary noting low recovery and acidic pH for sample AD29187, recommending re-extraction and re-analysis on January 4, 2002.
NYC-WTC_000036513–000036529Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\DEC1301\29187.D Vial: 6 Acq On : 13 Dec 2001 2:44 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 20 11:09 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 1168336 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 4452971 20.00 ug/1 -0.03 17) Acenaphthene-dlO 20.55 164 2199603 20.00 ug/1 -0.02 29) Phenanthrene-dlO 24.98 188 3163919 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1902387 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 1113720 20.00 ug/1 -0.02
System Monitoring Compounds 37) 2,4-DDD 30.05 235 112571 2.46 ug/mL -0.02 Spiked Amount 5.000 Recovery = 49.20%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.11 74 320 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.30 77 111 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 1380 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 19.97 163 176 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 20.57 153 101 N.D. 24) 2,4-Dinitrotoluene 21.27 165 180 N.D. 25) Diethylphthalate 22.07 149 2343 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 23.08 77 1406 N.D.
(#) = qualifier out of range (m) = manual integration 29187.D GCMS1126.M Fri Dec 21 13:01:26 2001 Page 1
NYC-WTC_000036515
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NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036530
Laboratory commentary confirming no unusual compounds detected in sample AD29521 during GCMS scan on January 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037457
Laboratory analysis report for environmental sample AD29929 showing GCMS results and surrogate compound recovery rates.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037040
Laboratory report of GCMS analysis for sample AD29784 conducted on January 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036995
Laboratory report of GCMS analysis for sample AD29787 conducted on January 7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035876
Lab notes for sample AD29087 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018123
Automated laboratory log recording GCMS analysis of sample AD30696 including detection of unknown compounds and surrogates.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049745
GCMS analysis report for sample AD31641 conducted on February 11, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036491
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036492
Fragmented page from a DEP environmental sampling record containing partial text and data fields.
Filed in the same folder
NYC-WTC_000036494
Laboratory calibration data sheet for GCMS analysis of organic compounds including nitrosamines and chlorobenzenes dated December 13, 2001.
Filed in the same folder
NYC-WTC_000036498
Laboratory report detailing GCMS calibration analysis for various organic compounds including nitrosamines and chlorobenzenes conducted on December 13, 2001.
Filed in the same folder
NYC-WTC_000036503
Laboratory report documenting GCMS blank analysis for organic compounds conducted on January 4, 2002, showing results below detection limits.
Filed in the same folder