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GCMS analysis data for sample AD29517, Jan 2002

Machine-extracted title · confidence 95%

Raw GCMS analysis data and chromatogram details for sample AD29517 including surrogate recovery results.

NYC-WTC_000036645–000036655

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1301\29466.D Vial: 12 Acq On : 13 Dec 2001 8:37 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 27 12:53 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 1213658 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 4597482 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 2264335 20.00 ug/1. -0.02 29) Phenanthrene-diO 24.97 188 3272561 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 2080977 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 1431834 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.05 235 119778 2.53 ug/mL -0.02 Spiked Amount 5.000 Recovery = 50.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl )ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane G . 00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 14.98 93 104 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 1265 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.33 165 116 N.D. 25) Diethylphthalate 22.09 149 1074 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 29466.D GCMS1126.M Thu Dec 27 12:56:41 2001 Page 1

NYC-WTC_000036647

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NYC-WTC_000036647Source: NYC Law Department, mirrored locally

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