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GCMS comments for sample AD29187, Jan 2002

Machine-extracted title · confidence 95%

Laboratory commentary noting low recovery and acidic pH for sample AD29187, recommending re-extraction and re-analysis on January 4, 2002.

NYC-WTC_000036513–000036529

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1301\29187.D Vial: 6 Acq On : 13 Dec 2001 2:44 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 20 11:09 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.04 178 1065 N.D. 34) Anthracene 25.19 178 571 N.D. 35) Di-n-butylphthalate 26.99 149 12208 N.D. 36) Fluoranthene 28.68 202 199 N.D. 39) Pyrene 29.34 202 321 N.D. 40) Butylbenzylphthalate 31.49 149 2131 N.D. 41) Benzo(a)anthracene 33.00 228 6871 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 33674 0.29 ug/1 93 43) Chrysene 33.00 228 6871 N.D. 45) Di-n-Octylphthalate 35.04 149 1305 N.D. 46) Benzo(b)fluoranthene 36.08 252 692 N.D. 47) Benzo(k)fluoranthene 36.13 252 1854 N.D. 48) Benzo(a)pyrene 36.93 252 258 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29187.D GCMS1126.M Fri Dec 21 13:01:30 2001 Page 2

NYC-WTC_000036516

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NYC-WTC_000036516Source: NYC Law Department, mirrored locally

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