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GCMS analysis comments for sample AD29464 with phthalate detection, Jan

Machine-extracted title · confidence 95%

Laboratory comments on GCMS scan results for sample AD29464 noting bis(2-Ethylhexyl)phthalate at 0.48 ug/L.

NYC-WTC_000036592–000036602

Folder label: “GCMS X 12/6/01 A 12/12/01 - 12/13/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1301\29518.D Vial: 10 Acq On : 13 Dec 2001 6:40 pm Operator: 209 GALOS Sample : gems scan 12/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 27 12:52 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D., 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.04 178 985 N.D. 34) Anthracene 25.04 178 985 N.D. 35) Di-n-butylphthalate 26.98 149 12296 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.49 149 3059 N.D. 41) Benzo(a)anthracene 33.01 228 4593 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 48480 0.44 ug/1 98 43) Chrysene 33.01 228 4593 N.D. ’45) Di-n-Octylphthalate 35.03 149 345 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.10 252 4675 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29518.D GCMS1126.M Thu Dec 27 12:57:56 2001 Page 2

NYC-WTC_000036595

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NYC-WTC_000036595Source: NYC Law Department, mirrored locally

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