GCMS calibration data for sample AD29522, Jan 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\ 1 \DATA\DEC3101 \CAL4 OB. D vial: 2 Acq On 2 Jan 2002 12:25 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 2 14:30 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) l,4-Dichlorobenzene-d4 11.68 152 1113356 20.00 ug/1 -0.02 10) Naphthalene-d8 15.29 136 4263538 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.57 164 2043192 20.00 ug/1 0.00 29) Phenanthrene-diO 24.99 188 3132589 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 2101224 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 1345829 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 29.90 235 23398 0.68 ug/mL -0.17 Spiked Amount 5.000 Recovery = 13.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.44 74 2141011m 43.72 ug/1 3) bis(2-Chloroethyl)ether 11.13 93 3263875 42.47 ug/1 92 4) 1,3-Dichlorobenzene 11.58 146 3138468 38.76 ug/1 99 5) 1,4-Dichlorobenzene 11.73 146 3181092 38.85 ug/1 98 6) 1,2-Dichlorobenzene 12.24 146 2903228 38.45 ug/1 98 7) 2,2' -oxybis (1-Chloropropan 12.58 45 5048280 < 51.58 ug/1 96 8) N-Nitroso-di-n-propylamine 12.99 70 2178403 49.75 ug/1 92 9) Hexachloroethane 13.07 117 1297160 43.56 ug/1 92 11) Nitrobenzene 13.37 77 3298240 49.63 ug/1 # 86 12) 1sophorone 14.02 82 6009485 46.94 ug/1 # 93 13) bis(2-Chloroethoxy)methane 14.71 93 3778778 43.93 ug/1 99 14) 1,2,4-Trichlorobenzene 15.18 180 2386073 38.54 ug/1 98 15) Naphthalene 15.35 128 8052017 39.52 ug/1 100 16) Hexachlorobutadiene 15.89 225 1229296 40.75 ug/1 99 18) Hexachlorocyclopentadiene 18.07 237 474296 32.22 ug/1 98 19) 2-Chloronaphthalene 18.84 162 4559075 39.11 ug/1 96 20) Dimethylphthalate 19.96 163 5339718 39.32 ug/1 100 21) 2,6-Dinitrotoluene 20.17 165 1286084 40.08 ug/1 # 59 2 2) Acenaphthylene 20.10 152 6451200 39.38 ug/1 100 2 3) Acenaphthene 20.67 153 4545341 38.81 ug/1 99 24) 2,4-Dinitrotoluene 21.35 165 1652650 40.52 ug/1 # 81 25) Diethylphthalate 22.10 149 5317587 42.32 ug/1 98 26) 4-Chlorophenyl-phenylether 22.21 204 2161076 39.40 ug/1 93 27) Fluorene 22.18 166 4687203 39.00 ug/1 99 28) Azobenzen/ 1,2-Diphenylhyd 22.69 77 6634144 C5210ug/u 90

(#) = qualifier out of range (m) = manual integration CAL40B.D GCMS1126.M Wed Jan 02 14:31:20 2002 Page 1

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